Α-(氯代二甲硅基)枯烯

产品名称 Α-(氯代二甲硅基)枯烯

CAS号118740-38-8

分子式C11H17ClSi

分子量212.79

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¹HNMR

¹³CNMR

IR1

Mass

MS-IW-3602          
chloro(alpha,alpha-dimethylbenzyl)dimethylsilane
C11H17ClSi          (Mass of molecular ion:    212)

   Source Temperature: 210 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      39.0       2.5
      41.0       8.5
      43.0       1.2
      51.0       2.3
      63.0       2.9
      65.0       5.0
      67.0       1.5
      73.0       2.6
      77.0       5.7
      78.0       3.6
      79.0       5.6
      91.0      32.8
      92.0       2.8
      93.0      32.0
      94.0       2.5
      95.0      11.4
     103.0       5.0
     104.0       1.1
     105.0       1.0
     115.0       2.0
     117.0       6.8
     118.0      52.7
     119.0     100.0
     120.0      10.1
     135.0       1.9
     155.0       2.7
     157.0       1.0
     177.0       1.1
     212.0      17.0
     213.0       2.9
     214.0       6.2
     215.0       1.0

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₁ H₁₇ Cl Si	0.05 ml : 0.5 ml CDCl₃
chloro(alpha,alpha-dimethylbenzyl)dimethylsilane

    Assign.     Shift(ppm)

      A             7.40
      B             7.39
      C             7.26
      D             1.577
      F             0.381
     
     CONFIRMED BY LAOCN PROGRAM.

     Hz     ppm     Int.

   2959.59   7.406    257
   2958.13   7.402    234
   2954.59   7.393    568
   2950.56   7.383     31
   2949.22   7.380     41
   2909.06   7.280     38
   2906.01   7.272     44
   2905.15   7.270     71
   2904.17   7.267     45
   2903.56   7.266     42
   2901.73   7.261     39
   2900.51   7.258     56
   2899.90   7.257     37
   2898.80   7.254     36
   2898.07   7.252     32
   2895.14   7.245     48
    633.54   1.586    123
    630.25   1.578    918
    626.71   1.569    112
    155.76   0.390    134
    152.47   0.382   1000
    149.05   0.373    123

in CDCl3

liquid film

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