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MS-NW-8561 N-ethyl-1-naphthylamine C12H13N (Mass of molecular ion: 171)
Source Temperature: 260 °C Sample Temperature: 140 °C Reservoir, 75 eV
27.0 2.2 28.0 5.2 29.0 1.3 39.0 3.8 42.0 3.1 50.0 2.7 51.0 5.2 52.0 1.3 62.0 2.5 63.0 7.4 64.0 2.9 65.0 4.7 74.0 3.0 75.0 4.9 76.0 2.8 77.0 11.4 78.0 7.3 83.0 1.6 85.0 1.6 86.0 1.3 87.0 2.2 88.0 2.1 89.0 5.4 101.0 4.0 102.0 2.1 113.0 2.8 114.0 3.8 115.0 29.2 116.0 5.1 117.0 1.2 126.0 7.0 127.0 19.7 128.0 29.8 129.0 48.6 130.0 5.8 140.0 3.2 141.0 2.2 142.0 3.5 143.0 3.3 153.0 1.7 154.0 14.8 155.0 8.0 156.0 100.0 157.0 12.4 167.0 1.7 168.0 2.0 169.0 1.4 170.0 8.1 171.0 80.1 172.0 10.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C12 H13 N 0.05 ml : 0.5 ml CDCl3 N-ethyl-1-naphthylamine Assign. Shift(ppm)
A 7.728 B 7.696 C 7.38 D 7.34 E 7.299 F 7.191 G 6.534 J 4.09 K 3.174 L 1.270
Hz ppm Int.
3093.63 7.741 165 3092.29 7.738 202 3084.47 7.718 210 3080.32 7.708 185 3079.59 7.706 178 3072.14 7.688 202 3071.41 7.686 193 2956.42 7.398 84 2955.08 7.395 106 2949.58 7.381 183 2948.36 7.378 209 2947.27 7.375 117 2941.89 7.362 192 2939.45 7.356 218 2937.62 7.351 209 2932.50 7.338 97 2930.91 7.334 197 2929.57 7.331 185 2926.03 7.322 190 2924.32 7.318 108 2922.73 7.314 96 2917.97 7.302 332 2910.28 7.283 260 2877.56 7.201 271 2869.38 7.180 195 2614.99 6.544 239 2607.42 6.525 228 1279.42 3.202 173 1272.34 3.184 491 1265.14 3.166 506 1258.06 3.148 186 519.78 1.301 36 514.77 1.289 565 507.32 1.270 1000 500.37 1.253 555
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