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MS-NW-6603 N-(hydroxymethyl)phthalimide C9H7NO3 (Mass of molecular ion: 177)
Source Temperature: 160 °C Sample Temperature: 100 °C Direct, 75 eV
18.0 2.0 28.0 6.2 29.0 18.6 30.0 15.6 37.0 4.1 37.5 1.0 38.0 5.5 39.0 1.6 45.5 2.7 49.0 1.8 50.0 22.8 51.0 2.2 52.0 4.4 59.5 2.7 61.0 1.1 62.0 1.0 63.0 1.7 64.0 1.4 66.0 6.1 73.0 2.3 73.5 1.0 74.0 10.1 75.0 9.5 76.0 55.4 77.0 5.2 90.0 2.4 92.0 1.1 102.0 1.2 103.0 17.2 104.0 62.3 105.0 6.8 130.0 3.7 147.0 100.0 148.0 12.0 149.0 2.6 160.0 1.1 177.0 4.8
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C9 H7 N O3 0.035 g : 0.5 ml DMSO-d6 N-(hydroxymethyl)phthalimide Assign. Shift(ppm)
A *1 7.921 B *1 7.885 C 6.44 D 4.989
Hz ppm Int.
3176.27 7.948 30 3175.05 7.945 45 3171.63 7.937 414 3168.70 7.929 385 3168.33 7.928 397 3166.75 7.924 376 3165.65 7.922 484 3162.84 7.915 852 3159.30 7.906 231 3158.69 7.904 231 3157.84 7.902 233 3157.35 7.901 248 3153.69 7.892 803 3151.00 7.885 430 3149.90 7.882 388 3148.32 7.878 389 3144.90 7.870 427 3141.60 7.861 52 3140.38 7.858 42 2580.20 6.457 215 2573.24 6.439 481 2566.16 6.422 233 1997.56 4.999 999 1990.48 4.981 1000
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