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网站主页CAS数据库列表 115570-52-0更多图谱新戊基乙二醇双(4-氨基苯基)醚(115570-52-0)质谱(MS)

新戊基乙二醇双(4-氨基苯基)醚

产品名称 新戊基乙二醇双(4-氨基苯基)醚

CAS号115570-52-0

分子式C17H22N2O2

分子量286.37


  • Mass

    MS-IW-8202          
    4,4'-(2,2-dimethyltrimethylenedioxy)dianiline
    C17H22N2O2          (Mass of molecular ion:    286)
    

       Source Temperature: 170 °C
       Sample Temperature: 150 °C
       Direct, 75 eV
    

          18.0       3.5
          27.0       1.1
          28.0       1.4
          29.0       1.0
          39.0       2.3
          41.0       4.2
          52.0       1.2
          53.0       2.8
          54.0       1.0
          55.0       2.0
          65.0       8.0
          66.0       1.3
          67.0       1.0
          69.0       6.4
          77.0       2.2
          80.0       7.5
          81.0       2.1
          91.0       1.0
          92.0       9.5
          93.0       3.9
          94.0       8.8
         106.0       1.6
         108.0      62.0
         109.0     100.0
         110.0      15.6
         111.0       1.1
         120.0       1.1
         121.0       2.7
         122.0      22.3
         123.0       1.9
         134.0       2.1
         136.0       1.1
         143.0       3.7
         148.0       2.0
         162.0       2.2
         177.0      50.6
         178.0      47.8
         179.0       5.7
         286.0      79.9
         287.0      16.1
         288.0       1.9
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C17 H22 N2 O2 0.037 g : 0.5 ml CDCl3
    4,4'-(2,2-dimethyltrimethylenedioxy)dianiline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.728 B 6.596 C 3.735 D 3.30 E 1.097

         Hz     ppm     Int.
    

       2697.75   6.751     25
       2694.34   6.742    238
       2692.02   6.736     86
       2687.74   6.726     94
       2685.42   6.720    343
       2682.01   6.711     44
       2643.55   6.615     39
       2640.14   6.607    337
       2637.82   6.601    102
       2633.54   6.590     87
       2631.23   6.584    254
       2627.81   6.576     31
       1492.80   3.736    658
       1319.58   3.302     48
        438.72   1.098   1000
    

in CDCl3



KBr disc



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