-
MassMS-NW-7572 5-amino-3-(p-chlorophenyl)-1,2,4-oxadiazole C8H6ClN3O (Mass of molecular ion: 195)
Source Temperature: 200 °C Sample Temperature: 130 °C Direct, 75 eV
27.0 1.1 28.0 3.0 30.0 1.6 37.0 2.0 38.0 2.4 39.0 2.8 43.0 1.6 44.0 10.1 49.0 1.3 50.0 10.0 51.0 6.0 52.0 1.8 61.0 2.2 62.0 5.2 63.0 7.9 64.0 2.6 73.0 5.0 74.0 6.3 75.0 19.1 76.0 6.4 77.0 1.0 83.0 1.0 84.0 1.0 85.0 2.1 86.0 1.9 87.0 2.8 88.0 3.6 89.0 4.9 90.0 22.4 91.0 1.8 97.0 1.3 98.0 2.5 99.0 2.1 100.0 2.3 101.0 1.3 102.0 14.1 103.0 2.0 110.0 1.2 111.0 10.2 112.0 1.5 113.0 3.5 117.0 2.2 123.0 3.1 124.0 1.5 125.0 22.6 126.0 2.1 127.0 7.4 137.0 16.5 138.0 15.2 139.0 6.9 140.0 5.4 152.0 57.9 153.0 39.9 154.0 22.3 155.0 13.5 156.0 1.4 165.0 1.0 195.0 100.0 196.0 10.4 197.0 33.5 198.0 3.6
400 MHz in DMSO-d6
-
1H NMR 399.65 MHz C8 H6 Cl N3 O 0.037 g : 0.5 ml DMSO-d6 5-amino-3-(p-chlorophenyl)-1,2,4-oxadiazole 
Assign. Shift(ppm)
A 8.02 B 7.903 C 7.582
Hz ppm Int.3224.12 8.068 30 3223.14 8.065 30 3222.29 8.063 32 3221.92 8.062 33 3221.56 8.061 34 3220.70 8.059 34 3220.21 8.058 39 3219.85 8.057 37 3218.63 8.054 42 3218.26 8.053 42 3217.77 8.052 44 3217.04 8.050 51 3216.43 8.049 55 3215.58 8.046 61 3214.11 8.043 73 3213.62 8.042 78 3204.22 8.018 913 3197.75 8.002 122 3196.17 7.998 79 3193.48 7.991 43 3192.99 7.990 40 3192.38 7.988 36 3191.89 7.987 37 3190.80 7.984 35 3190.31 7.983 31 3189.82 7.982 30 3174.93 7.945 33 3174.44 7.944 35 3174.07 7.943 33 3173.83 7.942 33 3173.10 7.940 39 3172.73 7.939 39 3171.88 7.937 41 3171.51 7.936 41 3170.53 7.934 49 3168.95 7.930 65 3168.21 7.928 74 3162.96 7.915 860 3161.25 7.911 389 3156.13 7.898 398 3154.42 7.893 1000 3148.80 7.879 43 3147.95 7.877 36 3043.95 7.617 30 3042.85 7.614 35 3042.11 7.612 39 3040.65 7.609 52 3039.67 7.606 67 3036.62 7.599 231 3034.18 7.593 977 3032.47 7.588 419 3027.59 7.576 373 3025.63 7.571 881 3018.19 7.553 34 3017.82 7.552 33 3016.97 7.550 30
in DMSO-d6
更多供应商