5-氨基-3-甲基-1-苯基吡唑

Mass

MS-IW-6471          
3-methyl-1-phenyl-5-pyrazolamine
C10H11N3            (Mass of molecular ion:    173)

   Source Temperature: 140 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      28.0       1.0
      39.0       2.0
      41.0       2.0
      42.0       1.4
      43.0       2.8
      51.0       3.2
      52.0       1.0
      64.0       1.5
      65.0       1.9
      66.0       1.8
      77.0       9.3
      78.0       2.0
      86.5       1.6
      91.0       3.5
      92.0       7.0
      93.0       1.5
     104.0       5.8
     105.0       1.5
     118.0       2.6
     119.0       2.0
     129.0       1.5
     130.0       6.8
     131.0       7.0
     132.0       2.9
     145.0       5.4
     155.0       9.3
     156.0       4.8
     157.0       3.0
     158.0       1.1
     172.0      29.5
     173.0     100.0
     174.0      12.6

Assign. Shift(ppm) A 7.518 B 7.433 C 7.299 D 5.413 E 3.8 F 2.216

     Hz     ppm     Int.

   3010.74   7.534    135
   3009.40   7.531    167
   3007.45   7.526     54
   3004.03   7.517     79
   3003.17   7.515    130
   3002.08   7.512    228
   3000.98   7.510    223
   2998.78   7.504     34
   2979.74   7.456     37
   2978.15   7.452    146
   2975.95   7.447     52
   2972.66   7.439     48
   2970.58   7.433    208
   2969.12   7.430    104
   2964.11   7.417     59
   2962.28   7.413    129
   2924.93   7.319     51
   2923.71   7.316     88
   2922.36   7.313     50
   2917.97   7.302     47
   2916.26   7.298    115
   2914.55   7.293     39
   2910.16   7.282     33
   2908.94   7.279     54
   2907.59   7.276     32
   2163.70   5.414    321
   1519.90   3.804     31
    886.11   2.218   1000