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MS-IW-0821 p-nitrobenzaldehyde oxime C7H6N2O3 (Mass of molecular ion: 166)
Source Temperature: 130 °C Sample Temperature: 110 °C Direct, 75 eV
17.0 1.1 18.0 6.0 27.0 1.5 28.0 4.3 30.0 5.4 38.0 1.6 39.0 11.9 44.0 1.1 50.0 13.4 51.0 9.5 52.0 3.0 53.0 4.9 62.0 2.2 63.0 8.0 64.0 5.1 65.0 29.2 66.0 2.6 74.0 4.8 75.0 21.2 76.0 21.6 77.0 8.8 78.0 1.2 80.0 1.0 81.0 6.4 89.0 2.8 90.0 5.4 91.0 5.2 92.0 8.2 93.0 7.0 102.0 20.4 103.0 13.1 104.0 2.5 109.0 1.1 118.0 4.7 119.0 8.8 120.0 6.2 123.0 2.0 136.0 11.5 137.0 1.0 139.0 3.1 148.0 10.2 149.0 4.6 150.0 5.6 166.0 100.0 167.0 9.4 168.0 1.0
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C7 H6 N2 O3 0.037 g : 0.5 ml DMSO-d6 p-nitrobenzaldehyde oxime Assign. Shift(ppm)
A 11.9 B 8.329 C 8.267 D 7.877
Hz ppm Int.
4753.72 11.895 96 4753.35 11.894 96 3329.05 8.330 1000 3317.51 8.302 23 3311.28 8.286 107 3309.09 8.280 802 3307.07 8.275 279 3302.13 8.263 281 3300.11 8.258 922 3297.91 8.252 147 3155.04 7.895 121 3152.66 7.889 831 3150.83 7.884 283 3148.27 7.878 46 3145.70 7.872 253 3143.69 7.867 759 3141.49 7.861 119
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