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网站主页CAS数据库列表 1122-81-2更多图谱4-丙基吡啶(1122-81-2)核磁图(13CNMR)

4-丙基吡啶

产品名称 4-丙基吡啶

CAS号1122-81-2

分子式C8H11N

分子量121.18

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  • Mass

    MS-NW-1017          
    4-propylpyridine
    C8H11N              (Mass of molecular ion:    121)
    

       Source Temperature: 260 °C
       Sample Temperature: 130 °C
       Reservoir, 75 eV
    

          18.0       1.3
          26.0       2.2
          27.0       8.5
          28.0       3.2
          29.0       8.9
          37.0       1.1
          38.0       3.1
          39.0      22.4
          40.0       2.8
          41.0       6.2
          42.0       2.1
          43.0       2.4
          50.0       5.3
          51.0      13.0
          52.0       9.0
          53.0       3.7
          54.0       3.4
          57.0       1.1
          62.0       1.5
          63.0       4.4
          64.0       2.6
          65.0      25.8
          66.0       8.5
          67.0       4.0
          77.0       5.8
          78.0       5.2
          79.0      11.7
          80.0       3.6
          91.0       3.8
          92.0      50.2
          93.0     100.0
          94.0       8.6
         104.0       1.6
         106.0      43.7
         107.0       5.0
         118.0       1.9
         120.0       9.8
         121.0      95.0
         122.0       8.6
    

90 MHz in CDCl3

400 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C8 H11 N 0.04 ml : 0.5 ml CDCl3
    4-propylpyridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.483 B 7.098 C 2.571 D 1.67 E 0.95

         Hz     ppm     Int.
    

        762.82   8.518    497
        761.23   8.500    310
        758.42   8.469    323
        756.84   8.451    566
        638.55   7.130    494
        636.96   7.113    292
        634.16   7.081    295
        632.57   7.064    451
        238.65   2.665    196
        231.57   2.586    393
        223.63   2.497    310
        159.67   1.783    168
        153.32   1.712    185
        152.71   1.706    185
        151.98   1.697    199
        151.37   1.691    146
        146.12   1.632    175
        144.41   1.613    241
        137.21   1.533    183
         91.55   1.023    584
         84.72   0.946   1000
         77.15   0.862    342
         76.17   0.851    191
    


  • 1H NMR 399.65 MHz
    C8 H11 N 14.5 mg : 0.5 ml CDCl3
    4-propylpyridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.483 B 7.102 C 2.581 D 1.661 E 0.950

         Hz     ppm     Int.
    

       3393.31   8.491    577
       3391.72   8.487    362
       3388.92   8.480    381
       3387.21   8.476    601
       3381.96   8.463     30
       2841.19   7.110    608
       2840.58   7.108    390
       2839.60   7.106    374
       2838.99   7.104    226
       2836.79   7.099    402
       2835.21   7.095    598
       1039.18   2.601    169
       1031.74   2.582    218
       1023.93   2.563    184
        682.98   1.709     43
        675.54   1.691    147
        674.44   1.688     32
        668.09   1.672    208
        666.99   1.669     83
        661.74   1.656     86
        660.52   1.653    237
        654.42   1.638     37
        652.95   1.634    151
        645.75   1.616     47
        386.84   0.968    484
        379.52   0.950   1000
        377.20   0.944     43
        372.19   0.932    437
    

in CDCl3



CCl4 solution



liquid film