-
MS-IW-7548 6-methyl-2-pyridinecarbaldehyde C7H7NO (Mass of molecular ion: 121)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
26.0 1.1 27.0 2.1 28.0 2.1 29.0 2.0 37.0 2.1 38.0 4.0 39.0 18.1 40.0 4.0 41.0 2.7 42.0 1.4 50.0 4.2 51.0 6.3 52.0 4.8 53.0 2.7 54.0 1.4 61.0 1.1 62.0 1.9 63.0 5.4 64.0 5.2 65.0 37.5 66.0 44.5 67.0 5.6 78.0 7.5 79.0 1.0 91.0 2.9 92.0 39.0 93.0 100.0 94.0 7.3 121.0 27.3 122.0 3.6
400 MHz in CDCl3
-
1H NMR 399.65 MHz C7 H7 N O 0.038 g : 0.5 ml CDCl3 6-methyl-2-pyridinecarbaldehyde Assign. Shift(ppm)
A 10.050 B 7.78 C 7.77 D 7.400 E 2.668
Hz ppm Int.
4016.88 10.051 309 4016.27 10.050 392 3115.54 7.796 32 3110.50 7.784 362 3107.91 7.777 150 3107.45 7.776 151 3104.55 7.769 136 3103.94 7.767 138 3096.92 7.750 28 3096.31 7.748 30 2962.04 7.412 86 2961.58 7.411 89 2959.29 7.405 60 2958.83 7.404 58 2955.78 7.396 92 2953.19 7.390 80 2952.73 7.389 82 1066.44 2.669 1000
更多供应商