-
MassMS-IW-9733 4-chloropyridine 1-oxide C5H4ClNO (Mass of molecular ion: 129)
Source Temperature: 150 °C Sample Temperature: 100 °C Direct, 75 eV
26.0 1.1 28.0 3.2 29.0 1.6 30.0 1.1 37.0 3.1 38.0 7.9 39.0 18.1 40.0 1.1 41.0 1.5 49.0 3.1 50.0 6.8 51.0 8.1 52.0 1.2 60.0 1.1 61.0 2.8 62.0 4.7 63.0 6.9 64.0 2.3 64.5 7.5 65.0 1.6 65.5 2.4 66.0 6.0 67.0 7.8 72.0 1.1 73.0 14.9 74.0 5.4 75.0 6.1 76.0 7.8 78.0 7.0 85.0 1.1 94.0 1.8 100.0 2.3 102.0 9.4 104.0 2.8 112.0 5.1 113.0 6.0 114.0 2.0 115.0 1.9 128.0 1.5 129.0 100.0 130.0 6.8 131.0 32.6 132.0 2.1
400 MHz in DMSO-d6
-
1H NMR 399.65 MHz C5 H4 Cl N O 0.041 g : 0.5 ml DMSO-d6 4-chloropyridine 1-oxide 
Assign. Shift(ppm)
A 8.283 B 7.587
Hz ppm Int.3316.04 8.298 110 3312.87 8.290 875 3310.91 8.285 383 3307.62 8.277 368 3305.66 8.272 933 3302.49 8.264 113 3039.06 7.605 120 3035.89 7.597 1000 3033.69 7.591 408 3030.52 7.583 380 3028.44 7.578 935 3025.27 7.570 108
in DMSO-d6
KBr disc
nujol mull
更多供应商
