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MS-NW-2665 1-tetradecanol C14H30O (Mass of molecular ion: 214)
Source Temperature: 270 °C Sample Temperature: 180 °C Reservoir, 75 eV
18.0 1.1 27.0 11.8 28.0 2.4 29.0 26.5 31.0 13.0 39.0 7.7 40.0 1.6 41.0 59.8 42.0 20.6 43.0 92.8 44.0 3.4 45.0 2.0 53.0 3.1 54.0 9.1 55.0 96.9 56.0 71.3 57.0 79.5 58.0 3.6 66.0 1.1 67.0 12.6 68.0 40.3 69.0 95.4 70.0 72.2 71.0 36.0 72.0 2.0 73.0 2.9 81.0 6.3 82.0 40.0 83.0 100.0 84.0 51.8 85.0 19.1 86.0 1.1 95.0 2.9 96.0 12.6 97.0 64.0 98.0 29.6 99.0 3.7 109.0 1.0 110.0 5.2 111.0 31.1 112.0 18.2 113.0 2.2 124.0 2.7 125.0 14.3 126.0 12.1 127.0 1.5 138.0 1.3 139.0 4.9 140.0 7.1 153.0 1.8 154.0 2.6 168.0 11.8 169.0 1.5 196.0 4.5
90 MHz in CDCl3
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1H NMR 89.56 MHz C14 H30 O 0.040 g : 0.5 ml CDCl3 1-tetradecanol Assign. Shift(ppm)
A 0.88 B 1.26 C 1.53 D 1.56 E 3.63
Hz ppm Int.
325.31 3.633 92 319.00 3.562 44 139.31 1.556 50 138.00 1.541 39 136.94 1.530 44 136.31 1.522 46 135.63 1.515 45 135.25 1.511 46 134.38 1.501 40 133.19 1.488 37 126.13 1.409 37 125.75 1.405 36 125.25 1.399 35 124.69 1.393 35 124.38 1.389 34 123.75 1.382 36 123.06 1.375 37 122.69 1.370 40 112.81 1.260 1000 78.81 0.880 93
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