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MS-NW-1221 1,2-bis(2-chloroethoxy)ethane C6H12Cl2O2 (Mass of molecular ion: 186)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 4.3 19.0 1.1 26.0 2.3 27.0 41.4 28.0 8.3 29.0 5.6 31.0 9.9 43.0 18.1 44.0 4.3 45.0 26.0 49.0 3.2 51.0 1.0 57.0 1.0 58.0 1.0 59.0 7.4 62.0 3.4 63.0 100.0 64.0 3.2 65.0 31.8 72.0 2.8 73.0 10.6 93.0 48.9 94.0 1.6 95.0 15.3 101.0 1.3 106.0 12.6 107.0 21.9 108.0 5.0 109.0 6.9 137.0 4.8 139.0 1.5
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H12 Cl2 O2 0.02 ml : 0.5 ml CDCl3 1,2-bis(2-chloroethoxy)ethane Assign. Shift(ppm)
A 3.76 B 3.694 C 3.66
Hz ppm Int.
346.00 3.864 32 343.00 3.830 55 342.31 3.823 38 337.94 3.774 181 337.50 3.769 130 334.25 3.733 180 333.38 3.723 217 330.81 3.694 1000 329.50 3.680 230 326.25 3.643 137 325.81 3.638 188 321.44 3.590 37 320.69 3.581 57 317.69 3.548 32
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