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MS-NW-9769 N,N'-diethyl-2-butene-1,4-diamine C8H18N2 (Mass of molecular ion: 142)
Source Temperature: 210 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.0 18.0 4.1 27.0 7.6 28.0 31.6 29.0 12.8 30.0 30.0 39.0 6.3 40.0 1.4 41.0 13.7 42.0 9.4 43.0 11.0 44.0 24.4 45.0 3.8 46.0 3.1 53.0 5.9 54.0 9.0 55.0 15.8 56.0 56.0 57.0 5.6 58.0 59.8 59.0 2.4 63.0 2.0 67.0 4.8 68.0 24.9 69.0 5.9 70.0 14.7 71.0 2.1 80.0 6.9 81.0 1.6 82.0 62.8 83.0 4.5 84.0 24.1 85.0 3.2 94.0 1.3 95.0 4.5 96.0 12.7 97.0 100.0 98.0 52.5 99.0 14.3 112.0 1.9 127.0 1.5 143.0 1.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H18 N2 0.05 ml : 0.5 ml CDCl3 N,N'-diethyl-2-butene-1,4-diamine Assign. Shift(ppm)
A 5.69 B 3.225 C 2.640 D 1.104
Hz ppm Int.
291.25 3.253 396 289.75 3.236 274 288.00 3.216 267 286.50 3.199 390 247.88 2.768 111 240.63 2.687 380 233.50 2.608 416 226.50 2.530 159 105.69 1.181 466 98.56 1.101 1000 91.50 1.022 375