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MS-NW-1373 3-hexenedinitrile C6H6N2 (Mass of molecular ion: 106)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 1.0 26.0 5.4 27.0 6.0 28.0 3.4 37.0 4.2 38.0 5.0 39.0 26.7 40.0 5.6 41.0 4.2 50.0 3.6 51.0 7.8 52.0 14.8 53.0 10.1 54.0 6.8 63.0 1.2 64.0 4.9 66.0 100.0 67.0 4.9 75.0 1.5 76.0 1.8 77.0 1.6 78.0 4.8 79.0 17.8 80.0 1.4 105.0 1.8 106.0 19.9 107.0 1.5
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H6 N2 0.047 g : 0.5 ml CDCl3 3-hexenedinitrile Assign. Shift(ppm)
A 5.828 B 3.188
Hz ppm Int.
525.50 5.868 129 524.56 5.858 197 522.88 5.839 226 521.94 5.828 405 521.00 5.818 224 519.44 5.800 222 518.50 5.790 128 287.31 3.209 1000 286.31 3.197 507 285.63 3.190 389 284.81 3.181 468 283.81 3.169 1000 281.56 3.144 41 281.00 3.138 36 280.31 3.130 29 280.19 3.129 29 279.75 3.124 30
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