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MS-IW-7345 2-methyl-1-naphthylamine hydrochloride C11H11N HCl (Mass of molecular ion: 157)
Source Temperature: 150 °C Sample Temperature: 130 °C Direct, 75 eV
36.0 8.9 38.0 3.0 51.0 1.6 63.0 1.8 64.0 2.1 64.5 1.1 65.0 3.7 65.5 4.3 76.5 1.5 77.0 4.5 77.5 3.8 78.0 5.4 78.5 8.8 79.0 1.1 115.0 2.3 116.0 1.7 126.0 1.0 127.0 5.9 128.0 10.6 129.0 12.4 130.0 2.7 139.0 3.6 140.0 4.2 141.0 3.5 154.0 2.6 156.0 61.6 157.0 100.0 158.0 12.0
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C11 H11 N 0.040 g : 0.5 ml DMSO-d6 2-methyl-1-naphthylamine hydrochloride Assign. Shift(ppm)
A 8.364 B 7.968 C *1 7.846 D 7.632 E 7.556 F *1 7.434 G 2.295
Hz ppm Int.
3348.65 8.379 121 3340.59 8.359 127 3340.04 8.358 128 3188.75 7.979 117 3181.05 7.960 128 3138.74 7.854 150 3130.32 7.833 167 3059.43 7.656 58 3057.96 7.652 64 3052.47 7.638 98 3051.00 7.635 124 3049.54 7.631 69 3044.04 7.617 91 3042.58 7.614 84 3027.19 7.575 93 3026.28 7.573 99 3019.13 7.555 131 3018.22 7.553 101 3012.17 7.538 62 3011.26 7.535 59 2975.36 7.445 206 2966.75 7.424 187 1037.46 2.596 1000
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