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MS-NW-1305 3,3'-iminodipropionitrile C6H9N3 (Mass of molecular ion: 123)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 3.6 18.0 1.5 26.0 7.5 27.0 8.8 28.0 23.6 29.0 3.8 30.0 23.4 38.0 1.2 39.0 1.9 40.0 5.1 41.0 6.9 42.0 95.7 43.0 11.6 51.0 3.0 52.0 8.1 53.0 6.2 54.0 52.2 55.0 4.7 56.0 4.8 57.0 1.0 66.0 1.1 67.0 1.4 81.0 6.1 82.0 3.0 83.0 100.0 84.0 5.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H9 N3 0.04 ml : 0.5 ml CDCl3 3,3'-iminodipropionitrile Assign. Shift(ppm)
A 2.96 B 2.54 C 1.54
Hz ppm Int.
273.13 3.050 238 272.00 3.038 258 270.06 3.016 37 265.56 2.966 890 259.94 2.903 502 259.31 2.896 531 233.38 2.606 512 232.63 2.598 554 229.69 2.565 38 228.44 2.551 42 227.13 2.537 1000 226.44 2.529 448 225.69 2.520 377 222.19 2.481 42 220.69 2.465 276 219.50 2.451 271 137.81 1.539 100
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