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MS-NW-0921 1,4-dibromobutane C4H8Br2 (Mass of molecular ion: 214)
Source Temperature: 290 °C Sample Temperature: 150 °C Reservoir, 75 eV
26.0 6.9 27.0 39.5 28.0 9.5 29.0 27.1 38.0 2.0 39.0 16.9 40.0 1.3 41.0 15.2 42.0 1.0 50.0 1.8 51.0 2.0 53.0 7.0 54.0 2.4 55.0 100.0 56.0 5.1 79.0 1.1 80.0 1.4 81.0 1.2 82.0 1.2 93.0 2.1 95.0 2.1 106.0 2.1 107.0 6.9 108.0 2.2 109.0 6.2 134.0 3.8 135.0 41.9 136.0 5.7 137.0 39.9 138.0 1.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C4 H8 Br2 0.05 ml : 0.5 ml CDCl3 1,4-dibromobutane Assign. Shift(ppm)
A 3.449 B 2.033
Hz ppm Int.
1384.89 3.466 470 1383.67 3.463 352 1382.45 3.460 323 1381.10 3.456 425 1379.76 3.453 455 1378.66 3.450 890 1377.44 3.447 469 1376.22 3.444 420 1374.76 3.440 312 1373.54 3.437 327 1372.31 3.434 461 821.53 2.056 142 818.60 2.049 452 817.38 2.046 304 815.80 2.042 452 815.19 2.040 431 813.60 2.036 380 812.38 2.033 1000 811.16 2.030 353 809.45 2.026 394 808.84 2.024 424 807.25 2.020 255 806.03 2.017 392
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