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MassMS-NW-0420 diethyl sebacate C14H26O4 (Mass of molecular ion: 258)
Source Temperature: 130 °C Sample Temperature: 90 °C Direct, 75 eV
18.0 1.8 26.0 1.0 27.0 12.4 28.0 6.3 29.0 41.9 30.0 1.0 31.0 1.6 39.0 5.8 40.0 1.5 41.0 33.0 42.0 9.1 43.0 14.9 45.0 11.9 53.0 3.0 54.0 4.1 55.0 47.3 56.0 9.9 57.0 4.7 59.0 4.0 60.0 21.1 61.0 16.6 67.0 8.5 68.0 5.0 69.0 25.5 70.0 16.3 71.0 3.5 73.0 14.1 74.0 2.3 79.0 3.7 80.0 3.1 81.0 9.5 82.0 3.6 83.0 19.7 84.0 30.8 85.0 2.8 87.0 4.5 88.0 44.8 89.0 4.6 91.0 1.0 93.0 3.6 94.0 2.7 95.0 8.5 96.0 6.7 97.0 34.9 98.0 53.9 99.0 4.4 101.0 26.8 102.0 3.1 107.0 4.3 109.0 2.3 110.0 5.1 111.0 8.2 112.0 6.3 113.0 1.0 115.0 7.2 116.0 1.7 119.0 2.2 120.0 2.3 121.0 11.6 122.0 1.7 123.0 2.2 124.0 10.2 125.0 60.2 126.0 5.4 127.0 1.2 128.0 2.2 129.0 15.0 130.0 2.4 137.0 3.0 138.0 28.7 139.0 20.3 140.0 2.2 141.0 1.0 143.0 5.0 144.0 1.3 148.0 5.4 149.0 2.7 155.0 1.1 156.0 2.2 157.0 3.0 158.0 11.2 159.0 1.2 165.0 1.5 166.0 40.3 167.0 8.4 168.0 2.3 169.0 1.5 170.0 11.8 171.0 95.3 172.0 10.8 173.0 1.0 184.0 11.8 185.0 5.0 186.0 11.4 187.0 1.5 194.0 1.0 212.0 15.8 213.0 100.0 214.0 13.6 215.0 1.8 258.0 2.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C14 H26 O4 0.04 ml : 0.5 ml CDCl3 diethyl sebacate 
Assign. Shift(ppm)
A 4.119 B 2.27 C 1.61 D 1.43 to 1.20 E 1.251
Hz ppm Int.379.94 4.243 104 372.75 4.163 358 365.63 4.083 379 358.56 4.004 127 212.25 2.370 59 211.25 2.359 60 204.63 2.285 171 197.13 2.202 146 151.56 1.693 39 151.00 1.687 38 149.94 1.675 37 149.25 1.667 35 148.25 1.656 34 147.63 1.649 37 146.00 1.631 47 145.38 1.624 51 144.25 1.611 54 143.69 1.605 54 143.38 1.601 54 142.81 1.595 52 140.69 1.571 42 140.19 1.566 41 139.44 1.557 42 138.94 1.552 43 138.44 1.546 42 137.94 1.541 42 137.63 1.537 42 137.13 1.532 41 136.69 1.527 41 136.19 1.521 41 130.63 1.459 30 130.25 1.455 30 125.31 1.400 39 119.06 1.330 589 116.75 1.304 340 112.06 1.252 1000 108.00 1.206 38 104.81 1.171 411
in CDCl3
CCl4 solution
liquid film
4880 A,200 M,liquid
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