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MS-NW-0822 trimethylenediamine C3H10N2 (Mass of molecular ion: 74)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.5 17.0 2.7 18.0 20.7 26.0 1.0 27.0 3.8 28.0 16.1 29.0 4.0 30.0 100.0 31.0 2.9 39.0 1.2 40.0 1.5 41.0 3.5 42.0 8.0 43.0 4.4 44.0 19.3 45.0 10.9 56.0 26.4 57.0 78.2 58.0 3.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C3 H10 N2 0.04 ml : 0.5 ml CDCl3 trimethylenediamine Assign. Shift(ppm)
A 2.761 B 1.591 C 1.15
Hz ppm Int.
254.63 2.844 393 247.81 2.767 964 240.94 2.691 534 156.25 1.745 98 155.38 1.735 101 149.19 1.666 357 148.25 1.656 184 142.13 1.587 423 135.69 1.516 210 135.06 1.509 242 128.75 1.438 64 127.88 1.428 65 102.75 1.148 1000
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