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网站主页CAS数据库列表 1087-02-1更多图谱1,4-二环己基苯(1087-02-1)核磁图(13CNMR)

1,4-二环己基苯

产品名称 1,4-二环己基苯

CAS号1087-02-1

分子式C18H26

分子量242.4

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  • Mass

    MS-NW-1266          
    p-dicyclohexylbenzene
    C18H26              (Mass of molecular ion:    242)
    

       Source Temperature: 260 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          27.0       2.4
          29.0       4.4
          39.0       3.4
          41.0      15.6
          43.0       1.8
          51.0       1.0
          53.0       2.5
          55.0      27.3
          56.0       1.6
          65.0       1.8
          67.0       4.3
          69.0       1.4
          77.0       2.9
          78.0       1.3
          79.0       2.1
          81.0       8.9
          82.0       3.4
          83.0      38.6
          84.0       2.5
          91.0      43.8
          92.0       5.6
          93.0       1.1
         103.0       1.6
         104.0       6.8
         105.0       4.6
         115.0       9.0
         116.0       3.2
         117.0      62.1
         118.0       7.5
         127.0       2.4
         128.0       8.8
         129.0      20.6
         130.0       8.9
         131.0       6.7
         141.0       2.7
         142.0       1.6
         143.0       9.3
         144.0       2.0
         145.0       1.1
         155.0       1.3
         157.0       2.5
         158.0       4.0
         159.0      62.4
         160.0      12.6
         161.0       1.0
         173.0      11.2
         174.0       2.0
         186.0      13.7
         187.0       2.7
         199.0       5.3
         200.0       2.0
         227.0       2.6
         242.0     100.0
         243.0      19.7
         244.0       1.9
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C18 H26 13.0 mg : 0.5 ml CDCl3
    p-dicyclohexylbenzene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.126 B 2.459 C 1.91 to 1.780 D 1.733 E 1.46 to 1.310 F 1.242

         Hz     ppm     Int.
    

       2847.78   7.126   1000
        983.52   2.461     34
        751.95   1.882     49
        750.00   1.877     49
        748.17   1.873     49
        747.07   1.870     50
        743.53   1.861     74
        742.68   1.859     74
        742.31   1.858     74
        739.75   1.851     59
        734.99   1.840     64
        734.01   1.837     61
        732.30   1.833     77
        730.22   1.828     60
        729.74   1.826     61
        726.44   1.818     60
        723.88   1.812     50
        723.63   1.811     50
        722.53   1.808     51
        698.85   1.749     32
        687.87   1.722     31
        686.40   1.718     33
        685.06   1.715     33
        568.48   1.423     49
        567.38   1.420     48
        566.04   1.417     50
        559.45   1.400     79
        558.59   1.398     79
        555.30   1.390    114
        551.03   1.379     90
        546.51   1.368     47
        545.53   1.366     53
        544.31   1.362     47
        542.11   1.357     57
        539.31   1.350     37
    

in CDCl3



KBr disc



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