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MS-IW-4925 (+)-2,10-camphorsultam C10H17NO2S (Mass of molecular ion: 215)
Source Temperature: 150 °C Sample Temperature: 110 °C Direct, 75 eV
15.0 1.4 27.0 12.1 28.0 18.1 29.0 8.8 30.0 14.2 39.0 20.2 40.0 4.9 41.0 43.7 42.0 9.3 43.0 48.7 44.0 20.6 45.0 2.3 50.0 1.1 51.0 4.5 52.0 3.3 53.0 16.2 54.0 8.9 55.0 21.0 56.0 13.2 57.0 5.2 58.0 3.7 59.5 1.0 60.5 1.0 63.0 1.5 64.0 2.1 65.0 7.2 66.0 5.4 67.0 31.9 68.0 24.6 69.0 26.6 70.0 12.1 71.0 2.2 77.0 15.0 78.0 3.8 79.0 19.2 80.0 12.0 81.0 18.0 82.0 52.1 83.0 67.0 84.0 6.4 85.0 6.4 86.0 1.7 91.0 24.4 92.0 7.2 93.0 72.6 94.0 36.6 95.0 30.6 96.0 21.4 97.0 3.2 105.0 8.1 106.0 8.5 107.0 15.8 108.0 100.0 109.0 23.8 110.0 17.3 111.0 1.7 117.0 1.5 119.0 75.1 120.0 9.4 121.0 3.9 122.0 21.4 123.0 8.7 124.0 1.3 132.0 14.8 133.0 3.0 134.0 71.9 135.0 11.2 136.0 85.9 137.0 8.9 149.0 1.5 150.0 15.5 151.0 84.7 152.0 9.7 215.0 2.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H17 N O2 S 0.042 g : 0.5 ml CDCl3 (+)-2,10-camphorsultam Assign. Shift(ppm)
A 4.35 B 3.428 C *1 3.126 D *1 3.108 E *2 1.987 F 1.92 to 1.88 G *2 1.85 J *3 1.459 K *3 1.311 L 1.133 M 0.934 ASSIGNED BY H-H COSY
Hz ppm Int.
1742.31 4.360 45 1736.08 4.345 45 1735.84 4.344 45 1380.49 3.455 48 1375.61 3.443 55 1372.44 3.435 71 1367.68 3.423 70 1364.87 3.416 54 1359.99 3.403 48 1261.60 3.157 47 1247.80 3.123 356 1243.90 3.113 400 1230.22 3.079 55 804.08 2.012 34 800.90 2.005 36 799.44 2.001 34 796.14 1.993 32 794.19 1.988 30 791.02 1.980 52 789.67 1.976 46 787.84 1.972 63 783.08 1.960 48 773.44 1.936 38 770.87 1.929 56 766.36 1.918 125 761.84 1.907 144 759.64 1.901 120 758.06 1.897 116 755.62 1.891 70 752.69 1.884 189 750.85 1.879 133 748.66 1.874 75 746.83 1.869 79 744.87 1.864 145 742.43 1.858 45 740.11 1.852 83 731.81 1.832 77 727.17 1.820 52 592.90 1.484 58 583.62 1.461 102 580.08 1.452 36 576.54 1.443 35 574.71 1.439 43 531.49 1.330 61 525.15 1.315 78 522.34 1.307 52 514.16 1.287 44 452.88 1.134 982 373.29 0.935 1000
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