L-(+)-樟脑内磺酰胺

Mass

MS-IW-4925          
(+)-2,10-camphorsultam
C10H17NO2S          (Mass of molecular ion:    215)

   Source Temperature: 150 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      15.0       1.4
      27.0      12.1
      28.0      18.1
      29.0       8.8
      30.0      14.2
      39.0      20.2
      40.0       4.9
      41.0      43.7
      42.0       9.3
      43.0      48.7
      44.0      20.6
      45.0       2.3
      50.0       1.1
      51.0       4.5
      52.0       3.3
      53.0      16.2
      54.0       8.9
      55.0      21.0
      56.0      13.2
      57.0       5.2
      58.0       3.7
      59.5       1.0
      60.5       1.0
      63.0       1.5
      64.0       2.1
      65.0       7.2
      66.0       5.4
      67.0      31.9
      68.0      24.6
      69.0      26.6
      70.0      12.1
      71.0       2.2
      77.0      15.0
      78.0       3.8
      79.0      19.2
      80.0      12.0
      81.0      18.0
      82.0      52.1
      83.0      67.0
      84.0       6.4
      85.0       6.4
      86.0       1.7
      91.0      24.4
      92.0       7.2
      93.0      72.6
      94.0      36.6
      95.0      30.6
      96.0      21.4
      97.0       3.2
     105.0       8.1
     106.0       8.5
     107.0      15.8
     108.0     100.0
     109.0      23.8
     110.0      17.3
     111.0       1.7
     117.0       1.5
     119.0      75.1
     120.0       9.4
     121.0       3.9
     122.0      21.4
     123.0       8.7
     124.0       1.3
     132.0      14.8
     133.0       3.0
     134.0      71.9
     135.0      11.2
     136.0      85.9
     137.0       8.9
     149.0       1.5
     150.0      15.5
     151.0      84.7
     152.0       9.7
     215.0       2.3

Assign. Shift(ppm) A 4.35 B 3.428 C *1 3.126 D *1 3.108 E *2 1.987 F 1.92 to 1.88 G *2 1.85 J *3 1.459 K *3 1.311 L 1.133 M 0.934 ASSIGNED BY H-H COSY

     Hz     ppm     Int.

   1742.31   4.360     45
   1736.08   4.345     45
   1735.84   4.344     45
   1380.49   3.455     48
   1375.61   3.443     55
   1372.44   3.435     71
   1367.68   3.423     70
   1364.87   3.416     54
   1359.99   3.403     48
   1261.60   3.157     47
   1247.80   3.123    356
   1243.90   3.113    400
   1230.22   3.079     55
    804.08   2.012     34
    800.90   2.005     36
    799.44   2.001     34
    796.14   1.993     32
    794.19   1.988     30
    791.02   1.980     52
    789.67   1.976     46
    787.84   1.972     63
    783.08   1.960     48
    773.44   1.936     38
    770.87   1.929     56
    766.36   1.918    125
    761.84   1.907    144
    759.64   1.901    120
    758.06   1.897    116
    755.62   1.891     70
    752.69   1.884    189
    750.85   1.879    133
    748.66   1.874     75
    746.83   1.869     79
    744.87   1.864    145
    742.43   1.858     45
    740.11   1.852     83
    731.81   1.832     77
    727.17   1.820     52
    592.90   1.484     58
    583.62   1.461    102
    580.08   1.452     36
    576.54   1.443     35
    574.71   1.439     43
    531.49   1.330     61
    525.15   1.315     78
    522.34   1.307     52
    514.16   1.287     44
    452.88   1.134    982
    373.29   0.935   1000