图谱信息 供应商 相关产品
网站主页CAS数据库列表 1083-48-3更多图谱4-(4-硝基苄基)吡啶(1083-48-3)质谱(MS)

4-(4-硝基苄基)吡啶

产品名称 4-(4-硝基苄基)吡啶

CAS号1083-48-3

分子式C12H10N2O2

分子量214.22

展开


  • Mass

    MS-NW-2324          
    4-(p-nitrobenzyl)pyridine
    C12H10N2O2          (Mass of molecular ion:    214)
    

       Source Temperature: 210 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          18.0       3.6
          27.0       1.5
          28.0       2.8
          30.0       3.9
          38.0       1.5
          39.0       9.7
          50.0       5.0
          51.0      10.1
          52.0       2.5
          54.0       2.3
          57.5       2.5
          62.0       2.6
          63.0       8.5
          64.0       2.6
          65.0       7.1
          69.5       1.3
          70.5       1.5
          74.0       1.7
          75.0       2.3
          76.0       1.9
          77.0       5.0
          78.0       4.8
          83.5       5.2
          84.0       1.6
          87.0       1.4
          88.0       1.1
          89.0       6.7
          90.0       2.9
          91.0       1.3
          92.0       2.7
         102.0       1.5
         106.0       2.3
         107.0       2.6
         113.0       1.4
         114.0       1.7
         115.0      10.7
         116.0       2.1
         117.0       1.6
         127.0       2.0
         128.0       3.2
         129.0       1.7
         139.0      11.1
         140.0       7.3
         141.0       7.5
         142.0       1.3
         154.0       2.5
         155.0       1.3
         156.0       7.2
         157.0       1.1
         166.0      10.2
         167.0      69.0
         168.0      45.1
         169.0       5.7
         183.0       1.3
         184.0       6.9
         197.0       4.6
         198.0       1.4
         213.0       2.5
         214.0     100.0
         215.0      14.0
         216.0       1.3
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C12 H10 N2 O2 0.046 g : 0.5 ml CDCl3
    4-(p-nitrobenzyl)pyridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.540 B 8.163 C 7.35 D 7.11 E 4.085

         Hz     ppm     Int.
    

        768.00   8.576    561
        766.38   8.558    361
        763.56   8.526    357
        761.94   8.508    642
        738.38   8.245     71
        735.94   8.218    603
        733.88   8.195    211
        729.19   8.142    205
        727.13   8.119    747
        724.69   8.092    106
        664.81   7.424     82
        664.13   7.416     63
        662.38   7.396    641
        660.31   7.373    195
        655.63   7.321    155
        653.50   7.297    568
        651.75   7.278     75
        651.13   7.271     78
        639.13   7.137    530
        638.50   7.130    363
        637.50   7.119    336
        634.75   7.088    309
        633.13   7.070    503
        365.88   4.086   1000
    

in CDCl3



CCl4 solution



KBr disc



nujol mull