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MassMS-NW-0045 m-xylene C8H10 (Mass of molecular ion: 106)
Source Temperature: 222 °C Sample Temperature: 55 °C Reservoir, 75 eV
27.0 2.7 28.0 1.3 38.0 1.2 39.0 7.7 41.0 1.2 50.0 2.7 51.0 7.5 52.0 3.4 53.0 2.1 62.0 1.6 63.0 4.7 65.0 6.0 74.0 1.1 77.0 11.3 78.0 5.6 79.0 7.1 89.0 1.9 91.0 100.0 92.0 7.6 102.0 1.1 103.0 6.0 104.0 2.6 105.0 28.8 106.0 71.0 107.0 6.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H10 0.05 ml : 0.5 ml CDCl3 m-xylene 
Assign. Shift(ppm)
A 7.109 B 6.96 C 6.94 D 2.278
Hz ppm Int.2849.49 7.130 58 2841.80 7.111 125 2834.47 7.093 81 2783.33 6.965 52 2781.25 6.960 122 2780.64 6.958 141 2779.91 6.956 146 2779.17 6.955 146 2778.44 6.953 165 2777.83 6.951 192 2777.22 6.950 203 2776.61 6.948 187 2769.90 6.931 140 2769.41 6.930 147 2768.68 6.928 139 2768.07 6.927 120 910.64 2.279 1000 910.28 2.278 994
in CDCl3
liquid film
4880 A,200 M,liquid
ANION RADICAL, REDUCTION WITH NA OR K IN DME
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