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MassMS-NW-6461 m-bromofluorobenzene C6H4BrF (Mass of molecular ion: 174)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
31.0 2.4 37.0 3.5 38.0 3.2 39.0 1.5 47.0 1.4 49.0 2.5 50.0 11.9 51.0 4.6 57.0 1.6 61.0 2.2 62.0 2.3 63.0 2.0 68.0 6.4 69.0 6.6 73.0 1.7 74.0 6.8 75.0 31.1 76.0 2.7 87.0 2.9 88.0 2.5 92.0 1.5 93.0 2.5 94.0 7.9 95.0 100.0 96.0 6.8 111.0 2.0 174.0 69.9 175.0 5.9 176.0 68.1 177.0 4.9 254.0 1.5
parameter in TMS
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1H NMR 300 MHz C6 H4 Br F 10 mol% in TMS m-bromofluorobenzene 
Parameter ppm Hz
D(A) 7.141 D(B) 6.856 D(C) 7.032 D(D) 7.163 J(A,B) 2.51 J(A,C) 0.24 J(A,D) 1.76 J(A,X) 8.38 J(B,C) 8.28 J(B,D) 0.90 J(B,X) 8.31 J(C,D) 8.06 J(C,X) 5.99 J(D,X) -0.46 LOEMKER,J.E. ET AL. J.PHYS.CHEM. 72, 991 (1968)
Hz ppm Int.2154.78 7.183 241 2153.10 7.177 387 2151.87 7.173 359 2148.65 7.162 308 2147.05 7.157 711 2146.12 7.154 857 2144.85 7.149 1000 2140.23 7.134 336 2138.43 7.128 395 2137.76 7.126 393 2136.03 7.120 279 2120.80 7.069 307 2118.26 7.061 50 2114.36 7.048 393 2112.49 7.042 446 2111.20 7.037 149 2106.23 7.021 438 2104.20 7.014 213 2098.46 6.995 266 2066.45 6.888 229 2065.42 6.885 236 2063.98 6.880 228 2062.95 6.876 216 2058.37 6.861 327 2057.08 6.857 347 2056.05 6.853 357 2054.72 6.849 359 2050.26 6.834 190 2049.04 6.830 172 2047.66 6.826 194 2046.47 6.822 155
liquid film
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