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网站主页CAS数据库列表 107264-00-6更多图谱1-氟-2,4,6-三甲基吡啶三氟甲烷磺酸盐(107264-00-6)红外图谱(IR2)

1-氟-2,4,6-三甲基吡啶三氟甲烷磺酸盐

产品名称 1-氟-2,4,6-三甲基吡啶三氟甲烷磺酸盐

CAS号107264-00-6

分子式C9H11F4NO3S

分子量289.25

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  • Mass

    MS-IW-5547          
    N-fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate
    C9H11F4NO3S         (Mass of molecular ion:    289)
    

       Source Temperature: 180 °C
       Sample Temperature: 190 °C
       Direct, 75 eV
    

          20.0       4.4
          27.0       2.1
          28.0       2.5
          39.0       6.3
          40.0       1.0
          41.0       2.2
          42.0       3.5
          48.0       1.8
          50.0       1.9
          51.0       4.2
          52.0       2.5
          53.0       3.9
          59.5       1.1
          63.0       1.8
          64.0       6.5
          65.0       4.9
          66.0       2.1
          67.0       1.2
          69.0      21.7
          77.0      11.2
          78.0       3.6
          79.0      25.7
          80.0       5.5
          81.0       2.4
          91.0       2.9
          92.0       1.3
          93.0       3.4
          94.0       1.7
          97.0       4.4
          98.0       1.5
         104.0       3.7
         105.0       1.0
         106.0      16.8
         107.0       2.6
         118.0       2.4
         119.0       1.4
         120.0      28.5
         121.0     100.0
         122.0      10.0
         124.0       2.4
         136.0       2.8
         138.0       4.7
         139.0      26.3
         140.0       3.5
         157.0       2.1
         269.0       3.6
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C9 H11 F4 N O3 S 0.038 g : 0.5 ml DMSO-d6
    N-fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.586 B 2.635 C 2.501

         Hz     ppm     Int.
    

       3032.10   7.587    232
       3031.62   7.586    237
       1053.34   2.636   1000
       1002.20   2.508     35
        999.51   2.501    513
    

KBr disc



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