-
MassMS-NW-0248 adipohydrazide C6H14N4O2 (Mass of molecular ion: 174)
Source Temperature: 210 °C Sample Temperature: 0 °C Direct, 75 eV
18.0 6.1 27.0 7.0 28.0 5.4 29.0 7.6 30.0 1.5 31.0 21.0 32.0 21.1 33.0 13.6 39.0 5.8 40.0 1.0 41.0 9.2 42.0 2.1 43.0 3.6 44.0 2.0 53.0 2.6 54.0 1.4 55.0 24.4 56.0 2.5 57.0 4.2 59.0 21.9 67.0 1.1 69.0 1.6 73.0 3.3 74.0 3.2 80.0 3.0 82.0 4.4 83.0 7.8 84.0 1.5 87.0 2.1 97.0 4.8 98.0 1.2 101.0 3.4 108.0 3.5 111.0 28.1 112.0 2.1 114.0 2.0 115.0 20.6 116.0 1.4 125.0 3.5 142.0 1.4 143.0 100.0 144.0 6.6 174.0 2.3
400 MHz in DMSO-d6
90 MHz in DMSO-d6
-
1H NMR 399.65 MHz C6 H14 N4 O2 saturated in DMSO-d6 adipohydrazide 
Assign. Shift(ppm)
A 8.93 B 4.15 C 1.991 D 1.443
Hz ppm Int.3569.95 8.933 562 1658.94 4.151 1000 801.85 2.007 432 801.09 2.005 432 795.75 1.992 896 789.79 1.977 447 577.09 1.444 914
-
1H NMR 89.56 MHz C6 H14 N4 O2 0.039 g : 0.5 ml DMSO-d6 adipohydrazide Assign. Shift(ppm)
A 8.89 B 4.14 C 2.00 D 1.46
Hz ppm Int.796.56 8.895 529 370.50 4.137 1000 185.56 2.072 271 185.13 2.068 270 184.31 2.058 266 179.38 2.003 831 173.38 1.936 429 170.25 1.901 150 169.88 1.897 146 136.69 1.527 371 133.19 1.488 483 130.13 1.453 813 127.06 1.419 423 126.81 1.416 423 124.06 1.386 247 123.75 1.382 248 120.50 1.346 89
DMSO-d6
KBr disc
nujol mull
更多供应商
