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MS-NW-4384 1,3-dibromobutane C4H8Br2 (Mass of molecular ion: 214)
Source Temperature: 240 °C Sample Temperature: 170 °C Reservoir, 75 eV
26.0 4.2 27.0 30.7 28.0 1.0 29.0 28.1 38.0 1.5 39.0 14.3 40.0 1.3 41.0 9.9 42.0 1.1 50.0 1.6 51.0 1.7 53.0 5.8 54.0 1.4 55.0 100.0 56.0 5.2 79.0 1.0 80.0 1.0 81.0 1.0 82.0 1.1 93.0 2.1 95.0 2.0 107.0 7.0 109.0 6.5 119.0 1.1 121.0 1.4 134.0 1.9 135.0 59.4 136.0 4.6 137.0 57.2 138.0 2.7 214.0 1.3 216.0 2.5 218.0 1.2
90 MHz in CDCl3
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1H NMR 89.56 MHz C4 H8 Br2 0.02 ml : 0.5 ml CDCl3 1,3-dibromobutane Assign. Shift(ppm)
A 4.31 B 3.552 C 2.27 D 1.757
Hz ppm Int.
324.94 3.629 196 319.13 3.564 356 318.19 3.553 226 317.56 3.546 234 311.94 3.484 261 208.00 2.323 112 206.25 2.303 165 204.94 2.289 146 200.19 2.236 116 199.44 2.227 165 160.69 1.795 1000 154.00 1.720 939
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