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MS-NW-9541 ethylphosphonic dichloride C2H5Cl2OP (Mass of molecular ion: 146)
Source Temperature: 240 °C Sample Temperature: 150 °C Reservoir, 75 eV
26.0 3.3 27.0 17.3 28.0 10.4 29.0 38.6 36.0 1.3 47.0 12.0 48.0 2.0 66.0 1.2 82.0 1.8 83.0 17.3 85.0 5.7 101.0 1.7 103.0 1.1 109.0 2.2 110.0 1.5 111.0 20.2 113.0 6.3 117.0 3.6 118.0 100.0 119.0 3.0 120.0 64.9 122.0 10.3 145.0 2.9 146.0 2.3 147.0 2.8 148.0 1.5 149.0 1.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C2 H5 Cl2 O P 0.05 ml : 0.5 ml CDCl3 ethylphosphonic dichloride Assign. Shift(ppm)
A 2.634 B 1.423 J(P-31,B)=30.0HZ J(P-31,A)=14.8HZ
Hz ppm Int.
1070.92 2.680 187 1063.35 2.661 519 1055.91 2.643 618 1048.46 2.624 634 1043.09 2.611 37 1041.02 2.605 531 1033.57 2.587 196 596.68 1.494 37 591.19 1.480 546 583.74 1.461 986 579.22 1.450 37 576.17 1.442 529 568.24 1.422 37 567.14 1.420 46 566.65 1.418 47 561.04 1.404 552 553.59 1.386 1000 548.22 1.372 46 546.02 1.367 533 540.77 1.354 33
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