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网站主页CAS数据库列表 106-53-6更多图谱4-溴苯硫酚(106-53-6)质谱(MS)

4-溴苯硫酚

产品名称 4-溴苯硫酚

CAS号106-53-6

分子式C6H5BrS

分子量189.07

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  • Mass

    MS-NW-3450          
    p-bromobenzenethiol
    C6H5BrS             (Mass of molecular ion:    188)
    

       Source Temperature: 220 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          37.0       2.3
          38.0       2.9
          39.0       4.4
          45.0       4.7
          49.0       1.1
          50.0       7.8
          51.0       3.0
          53.0       1.3
          54.0       6.6
          57.0       1.8
          58.0       3.0
          61.0       1.7
          62.0       2.7
          63.0       7.2
          64.0       1.4
          65.0      18.3
          66.0       1.0
          69.0      11.1
          73.0       1.2
          74.0       4.5
          75.0       5.5
          76.0       3.6
          77.0       1.2
          81.0       2.0
          82.0       5.4
          83.0       1.6
          94.0       2.6
          95.0       2.6
         107.0       1.3
         108.0      20.9
         109.0     100.0
         110.0       8.4
         111.0       4.9
         155.0       1.1
         157.0       1.0
         187.0       4.4
         188.0      57.4
         189.0       8.6
         190.0      58.3
         191.0       4.6
         192.0       2.6
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H5 Br S 0.050 g : 0.5 ml CDCl3
    p-bromobenzenethiol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.32 B 7.13 C 3.42

         Hz     ppm     Int.
    

        664.13   7.416     41
        661.94   7.392    412
        659.75   7.367    163
        655.44   7.319    242
        653.25   7.294   1000
        651.00   7.269    172
        649.63   7.254     30
        649.06   7.248     29
        643.56   7.186    135
        641.31   7.161    964
        639.13   7.137    240
        637.44   7.118     29
        634.81   7.089    141
        632.63   7.064    384
        630.44   7.040     51
        306.63   3.424    904
    

in CDCl3



KBr disc



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