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网站主页CAS数据库列表 10567-86-9更多图谱苯基硫代乙内酰脲-谷氨酰胺(10567-86-9)核磁图(1HNMR)

苯基硫代乙内酰脲-谷氨酰胺

产品名称 苯基硫代乙内酰脲-谷氨酰胺

CAS号10567-86-9

分子式C12H13N3O2S

分子量263.32

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  • Mass

    MS-NW-2059          
    5-(2-carbamoylethyl)-3-phenyl-2-thioxo-4-imidazolidone
    C12H13N3O2S         (Mass of molecular ion:    263)
    

       Source Temperature: 200 °C
       Sample Temperature: 240 °C
       Direct, 75 eV
    

          14.0       1.8
          15.0       1.8
          16.0       3.4
          17.0       5.4
          18.0      25.0
          26.0       8.2
          27.0      18.2
          28.0      21.4
          29.0       1.9
          30.0       2.0
          32.0       7.9
          33.0       3.4
          34.0      10.2
          37.0       3.4
          38.0       7.3
          39.0      19.9
          40.0       6.8
          41.0      21.4
          42.0       6.9
          43.0       7.6
          44.0      15.7
          45.0       3.6
          50.0      10.8
          51.0      34.4
          52.0      10.2
          53.0       7.9
          54.0      14.0
          55.0      14.9
          56.0       8.0
          57.0       1.8
          58.0       2.9
          59.0      39.4
          60.0       2.9
          61.0       1.4
          62.0       1.9
          63.0       6.5
          64.0       9.7
          65.0       9.7
          66.0       7.7
          67.0       2.9
          68.0       3.0
          69.0       1.9
          70.0       8.2
          71.0       2.4
          72.0       3.7
          73.0       4.4
          74.0       2.6
          75.0       3.4
          76.0       9.4
          77.0     100.0
          78.0      11.1
          79.0       1.4
          80.0       3.4
          81.0       4.0
          82.0       4.1
          83.0       6.9
          84.0       8.0
          85.0       6.9
          86.0      14.1
          87.0       1.5
          88.0       1.5
          89.0       1.6
          90.0       3.5
          91.0      13.5
          92.0       8.3
          93.0      34.8
          94.0       5.5
          95.0       3.6
          96.0       1.4
          97.0       1.7
          98.0       5.8
          99.0       6.1
         100.0       2.3
         101.0       1.2
         102.0       1.0
         103.0      17.7
         104.0      45.0
         105.0       9.7
         106.0       2.6
         108.0       9.6
         109.0      13.0
         110.0       2.4
         111.0      13.8
         112.0       4.2
         116.0       1.1
         117.0       7.3
         118.0       7.4
         119.0      14.3
         120.0      13.4
         121.0       1.4
         123.0       1.0
         124.0       1.4
         125.0       2.2
         126.0       4.6
         127.0       1.9
         128.0       2.0
         129.0       1.3
         130.0       4.0
         131.0       2.7
         132.0       2.5
         133.0       2.1
         134.0       1.7
         135.0      72.9
         136.0      33.2
         137.0       6.1
         138.0       1.7
         142.0       1.7
         143.0       2.1
         144.0       2.5
         145.0       4.9
         146.0       6.6
         147.0       1.8
         149.0       1.1
         150.0       1.4
         151.0       2.5
         156.0       1.3
         157.0       2.5
         158.0       2.5
         159.0       2.2
         160.0       4.2
         161.0       1.4
         162.0       1.1
         163.0       1.5
         168.0       1.5
         170.0       1.7
         171.0       1.4
         172.0       7.5
         173.0       3.0
         174.0       1.7
         175.0       3.3
         176.0       1.3
         184.0       2.4
         185.0       3.1
         186.0       6.7
         187.0       5.0
         188.0       2.2
         189.0       5.5
         190.0       1.2
         191.0       2.7
         192.0       7.6
         193.0       1.1
         201.0       1.2
         202.0       2.5
         203.0      24.2
         204.0      49.9
         205.0      25.1
         206.0       5.2
         207.0       1.3
         211.0       2.4
         212.0       3.2
         213.0       3.6
         214.0       6.5
         215.0       1.4
         216.0       6.4
         217.0       8.6
         218.0      21.0
         219.0       3.7
         220.0       1.7
         229.0       3.1
         230.0       1.1
         231.0       2.5
         242.0       1.4
         243.0       6.6
         244.0      16.3
         245.0      33.0
         246.0      59.4
         247.0       9.8
         248.0       3.5
         261.0       4.5
         263.0      51.2
         264.0       7.8
         265.0       3.0
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C12 H13 N3 O2 S 0.035 g : 0.5 ml DMSO-d6
    5-(2-carbamoylethyl)-3-phenyl-2-thioxo-4-imidazolidone
    ChemicalStructure
        Assign.     Shift(ppm)
    A 10.6 B 7.485 C 7.44 D *1 7.40 E 7.296 F *1 6.88 G 4.464 J *2 2.27 K *2 2.24 L *3 2.05 M *3 1.97

         Hz     ppm     Int.
    

       4228.95  10.582    472
       3001.37   7.510    167
       2999.90   7.507    306
       2998.25   7.503    159
       2992.94   7.489    812
       2991.29   7.485    475
       2986.90   7.474    308
       2985.43   7.471    763
       2978.47   7.453    227
       2977.01   7.450    452
       2975.72   7.446    320
       2972.43   7.438    155
       2969.86   7.432    457
       2966.93   7.424    124
       2963.82   7.417    125
       2962.53   7.413    188
       2961.25   7.410    156
       2956.31   7.398    245
       2920.96   7.309    660
       2919.49   7.306   1000
       2917.29   7.300    242
       2914.18   7.292    386
       2912.53   7.288    735
       2911.25   7.285    601
       2908.68   7.279     93
       2750.79   6.883    240
       1791.00   4.482    173
       1785.51   4.468    362
       1779.83   4.454    171
       1778.91   4.452    180
        919.50   2.301     36
        911.44   2.281    175
        908.32   2.273    179
        901.91   2.257    372
        899.90   2.252    276
        895.13   2.240    262
        893.30   2.236    279
        884.69   2.214     46
        837.07   2.095     53
        831.58   2.081     62
        829.01   2.075     85
        823.33   2.061    159
        816.01   2.042    149
        814.91   2.040    148
        809.23   2.025    130
        802.82   2.009    115
        796.59   1.994    166
        794.03   1.987    112
        789.81   1.977    146
        787.43   1.971    151
        782.49   1.958    110
        780.84   1.954    118
        775.71   1.941     62
        773.70   1.936     69
        766.92   1.919     31
    

in DMSO-d6



KBr disc