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MassMS-IW-0715 10-chloro-9-anthracenecarbaldehyde C15H9ClO (Mass of molecular ion: 240)
Source Temperature: 190 °C Sample Temperature: 140 °C Direct, 75 eV
62.0 1.1 74.0 2.2 75.0 6.3 75.5 1.3 76.0 1.3 87.0 5.8 87.5 3.6 88.0 18.4 88.5 4.1 93.0 4.8 94.0 1.6 98.0 1.4 99.0 1.2 102.0 1.7 102.5 1.2 105.0 1.5 105.5 2.3 106.0 8.8 106.5 2.0 107.0 2.8 120.0 3.0 121.0 1.1 149.0 2.2 150.0 5.3 151.0 4.2 174.0 5.8 175.0 7.4 176.0 43.4 177.0 20.8 178.0 3.0 205.0 40.4 206.0 7.0 210.0 1.3 211.0 18.7 212.0 33.9 213.0 10.8 214.0 11.0 215.0 1.6 239.0 48.9 240.0 100.0 241.0 31.4 242.0 33.2 243.0 5.1
400 MHz (at 60.C)
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1H NMR 399.65 MHz C15 H9 Cl O 0.037 g : 0.5 ml CDCl3 10-chloro-9-anthracenecarbaldehyde 
Assign. Shift(ppm)
A 11.361 B 8.810 C 8.512 D *1 7.61 E *1 7.56
Hz ppm Int.4540.70 11.362 1000 3525.59 8.822 521 3525.04 8.821 528 3521.74 8.813 49 3516.61 8.800 586 3407.08 8.526 491 3403.05 8.516 50 3399.02 8.505 551 3397.74 8.502 485 3049.17 7.630 214 3047.71 7.626 233 3042.58 7.614 450 3041.11 7.610 474 3038.92 7.604 226 3034.15 7.593 496 3032.32 7.588 476 3030.86 7.584 502 3029.39 7.581 517 3024.26 7.568 252 3022.06 7.562 482 3020.97 7.560 445 3015.47 7.546 258 3014.37 7.543 216
in CDCl3
KBr disc
nujol mull
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