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网站主页CAS数据库列表 105-31-7更多图谱1-己炔-3-醇(105-31-7)核磁图(1HNMR)

1-己炔-3-醇

产品名称 1-己炔-3-醇

CAS号105-31-7

分子式C6H10O

分子量98.14

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  • Mass

    MS-NW-3132          
    1-hexyn-3-ol
    C6H10O              (Mass of molecular ion:     98)
    

       Source Temperature: 280 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          15.0       1.5
          18.0       1.3
          26.0       3.6
          27.0      25.7
          28.0       3.4
          29.0       8.3
          31.0       1.5
          37.0       1.2
          38.0       3.1
          39.0      14.8
          40.0       2.3
          41.0      30.2
          42.0       7.3
          43.0      30.0
          44.0       2.4
          45.0       1.6
          50.0       2.8
          51.0       4.2
          52.0       3.7
          53.0       5.1
          54.0       2.3
          55.0     100.0
          56.0      18.4
          57.0       4.9
          65.0       2.1
          67.0       1.7
          68.0       1.1
          69.0      10.0
          70.0      14.3
          71.0       3.8
          72.0       1.2
          77.0       2.3
          79.0       9.4
          80.0       1.6
          81.0       1.0
          83.0      32.2
          84.0       2.0
          97.0       6.4
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H10 O 0.05 ml : 0.5 ml CDCl3
    1-hexyn-3-ol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.38 B 2.66 C 2.462 D 1.67 E 1.51 F 0.96 J(A,C)=2.1HZ. J(A,D)=6.3HZ.

         Hz     ppm     Int.
    

        399.75   4.464     67
        397.63   4.440     75
        396.56   4.428     30
        395.13   4.412     33
        393.50   4.394    166
        391.38   4.371    162
        387.06   4.322     99
        384.94   4.299     99
        240.13   2.682    139
        237.50   2.652    230
        221.56   2.474   1000
        220.56   2.463     61
        219.44   2.451    991
        163.00   1.821     59
        161.06   1.799     35
        159.56   1.782     48
        158.56   1.771     68
        158.13   1.766     73
        156.25   1.745    136
        154.00   1.720     95
        151.50   1.692    107
        150.06   1.676    191
        149.38   1.668    197
        148.88   1.663    174
        147.25   1.645    193
        145.56   1.626    120
        145.00   1.620    135
        143.88   1.607    240
        142.56   1.592    211
        141.50   1.580    136
        140.81   1.573     77
        139.44   1.557     95
        137.31   1.534    181
        135.31   1.511    135
        133.25   1.488     57
        132.63   1.481     89
        131.94   1.474     88
        131.38   1.467     72
        129.75   1.449     84
        128.69   1.437     90
        127.63   1.426     77
        126.50   1.413     56
        125.50   1.402     75
        122.31   1.366     67
        121.44   1.356     64
        115.38   1.289     38
        114.94   1.284     39
         94.19   1.052     42
         91.88   1.026    290
         91.19   1.019    281
         88.94   0.994     79
         88.31   0.987     71
         87.75   0.980     66
         85.19   0.952    738
         83.25   0.930    229
         81.56   0.911     67
         78.94   0.882    138
         77.75   0.869    148
         76.19   0.851     83
    

in CDCl3



liquid film