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MassMS-NW-0846 2-(diethylamino)ethyl methacrylate C10H19NO2 (Mass of molecular ion: 185)
Source Temperature: 280 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 2.5 28.0 6.4 29.0 4.6 30.0 6.6 32.0 1.0 39.0 2.9 41.0 8.2 42.0 4.7 43.0 2.2 44.0 2.4 56.0 4.3 57.0 2.0 58.0 7.7 69.0 5.1 70.0 1.5 71.0 1.7 72.0 1.0 84.0 2.4 86.0 100.0 87.0 5.8 99.0 4.9 100.0 1.7 113.0 8.0 185.0 1.2
90 MHz in CDCl3
400 MHz in CDCl3
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1H NMR 89.56 MHz C10 H19 N O2 0.04 ml : 0.5 ml CDCl3 2-(diethylamino)ethyl methacrylate 
Assign. Shift(ppm)
A 6.100 B 5.550 C 4.216 D 2.759 E 2.588 F 1.945 G 1.047 J(A,B)=1.6HZ J(A,F)=-1.0HZ J(B,F)=-1.6HZ
Hz ppm Int.548.56 6.126 37 547.63 6.115 99 546.63 6.104 122 545.88 6.096 124 544.94 6.085 99 544.06 6.075 35 500.19 5.585 31 498.63 5.568 113 497.00 5.550 164 495.38 5.532 106 384.25 4.291 154 377.88 4.220 347 371.75 4.151 193 253.19 2.828 180 246.94 2.758 330 244.75 2.733 30 243.19 2.716 113 240.69 2.688 155 235.81 2.633 418 233.81 2.611 39 228.69 2.554 455 226.69 2.532 37 221.88 2.478 151 175.44 1.959 371 174.44 1.948 466 173.88 1.942 445 172.88 1.931 366 170.94 1.909 32 100.44 1.122 488 98.44 1.100 42 93.44 1.044 1000 91.31 1.020 66 86.25 0.964 386
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1H NMR 399.65 MHz C10 H19 N O2 0.05 ml : 0.5 ml CDCl3 2-(diethylamino)ethyl methacrylate Assign. Shift(ppm)
A 6.107 B 5.559 C 4.226 D 2.772 E 2.605 F 1.946 G 1.052
Hz ppm Int.2443.36 6.114 57 2442.38 6.112 145 2441.28 6.109 171 2440.67 6.108 167 2439.58 6.105 149 2438.60 6.102 60 2225.10 5.568 48 2223.51 5.564 167 2221.92 5.560 238 2220.21 5.556 158 2218.63 5.552 48 1695.43 4.243 249 1689.21 4.227 498 1682.98 4.212 265 1114.14 2.788 230 1110.11 2.778 31 1107.91 2.773 425 1101.68 2.757 224 1052.12 2.633 213 1044.92 2.615 581 1037.72 2.597 580 1030.64 2.579 226 779.05 1.950 496 778.08 1.947 534 777.47 1.946 524 776.37 1.943 469 427.49 1.070 637 420.41 1.052 1000 413.21 1.034 600
in CDCl3
liquid film
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