图谱信息 供应商 相关产品
网站主页CAS数据库列表 104706-47-0更多图谱(R)-3-羟基吡咯烷盐酸盐(104706-47-0)质谱(MS)

(R)-3-羟基吡咯烷盐酸盐

产品名称 (R)-3-羟基吡咯烷盐酸盐

CAS号104706-47-0

分子式C4H10ClNO

分子量123.58

展开


  • Mass

    MS-IW-4172          
    (R)-3-pyrrolidinol hydrochloride
    C4H9NO HCl          (Mass of molecular ion:     87)
    

       Source Temperature: 180 °C
       Sample Temperature: 130 °C
       Direct, 75 eV
    

          15.0       3.9
          17.0       1.0
          18.0       6.3
          26.0       1.2
          27.0       5.6
          28.0      27.0
          29.0       9.4
          30.0      49.7
          31.0       5.7
          32.0       1.0
          35.0       7.3
          36.0      77.1
          37.0       2.6
          38.0      35.3
          39.0       5.0
          40.0       2.6
          41.0      15.2
          42.0      29.4
          43.0     100.0
          44.0      15.2
          56.0       3.3
          57.0       9.1
          58.0       2.9
          59.0      11.6
          67.0       1.2
          68.0       6.0
          69.0       1.7
          70.0       2.7
          72.0       1.9
          86.0       3.6
          87.0      65.7
          88.0       6.0
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C4 H9 N O 0.039 g : 0.5 ml DMSO-d6
    (R)-3-pyrrolidinol hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.49 B 5.42 C 4.39 D *1 3.21 E *1 3.18 F 3.132 G 3.008 J *2 1.89 K *2 1.86 ASSIGNED BY CH-COSY

         Hz     ppm     Int.
    

       3793.18   9.492    204
       2166.75   5.422    246
       1755.37   4.393    480
       1753.08   4.387    532
       1751.40   4.383    512
       1297.15   3.246     57
       1294.86   3.240     30
       1291.96   3.233    109
       1289.06   3.226    120
       1286.01   3.218    610
       1284.33   3.214    711
       1281.13   3.206    599
       1277.31   3.197   1000
       1275.63   3.192    702
       1273.04   3.186    624
       1267.85   3.173    517
       1263.89   3.163    146
       1260.83   3.155    501
       1256.56   3.145    584
       1248.93   3.126    747
       1244.51   3.115    723
       1207.12   3.021    775
       1195.07   2.991    513
        776.06   1.942     61
        771.79   1.932     57
        766.60   1.919     81
        762.79   1.909    299
        758.51   1.898    300
        753.63   1.886    675
        749.51   1.876    732
        747.53   1.871    560
        745.24   1.865    563
        741.12   1.855    511
        735.93   1.842    105
        734.41   1.838    101
    

in DMSO-d6



KBr disc



nujol mull