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MassMS-NW-0854 N,N-diethyltrimethylenediamine C7H18N2 (Mass of molecular ion: 130)
Source Temperature: 280 °C Sample Temperature: 150 °C Reservoir, 75 eV
18.0 1.5 27.0 4.4 28.0 7.9 29.0 6.6 30.0 24.4 41.0 3.5 42.0 8.4 43.0 2.2 44.0 8.5 54.0 1.0 56.0 8.9 57.0 5.2 58.0 27.7 59.0 1.3 70.0 2.3 71.0 1.3 72.0 42.6 73.0 2.4 74.0 3.9 84.0 2.8 85.0 1.5 86.0 100.0 87.0 6.3 98.0 3.3 100.0 3.5 101.0 2.6 113.0 5.2 130.0 9.8
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H18 N2 0.04 ml : 0.5 ml CDCl3 N,N-diethyltrimethylenediamine 
Assign. Shift(ppm)
A 2.723 B 2.501 C 2.49 D 1.59 E 1.47 F 1.021
Hz ppm Int.251.31 2.807 98 244.50 2.731 231 237.69 2.654 140 236.38 2.640 131 235.88 2.634 116 228.88 2.556 516 221.69 2.476 616 220.19 2.459 88 219.31 2.449 91 214.44 2.395 278 157.06 1.754 35 156.06 1.743 35 150.88 1.685 35 150.00 1.675 78 149.06 1.665 80 144.44 1.613 41 142.25 1.589 103 135.75 1.516 64 134.94 1.507 81 132.06 1.475 258 129.00 1.441 39 128.00 1.430 31 98.19 1.097 489 91.19 1.019 1000 83.94 0.938 380
in CDCl3
liquid film
4880 A,100M,liquid
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