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网站主页CAS数据库列表 104-74-5更多图谱十二烷基氯化吡啶(104-74-5)质谱(MS)

十二烷基氯化吡啶

产品名称 十二烷基氯化吡啶

CAS号104-74-5

分子式C17H30ClN

分子量283.88

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  • Mass

    MS-NW-7902          
    1-dodecylpyridinium chloride
    C17H30ClN           (Mass of molecular ion:    283)
    

       Source Temperature: 210 °C
       Sample Temperature: 220 °C
       Direct, 75 eV
    

          18.0       1.7
          26.0       4.8
          27.0      14.8
          28.0       3.9
          29.0      25.9
          36.0       3.2
          37.0       1.2
          38.0       1.8
          39.0      13.8
          40.0       2.0
          41.0      51.8
          42.0      15.0
          43.0     100.0
          44.0       3.4
          49.0       2.4
          50.0      10.1
          51.0      15.9
          52.0      38.6
          53.0       7.5
          54.0       4.0
          55.0      52.4
          56.0      21.0
          57.0      91.4
          58.0       4.2
          63.0       2.1
          67.0       4.0
          68.0       3.6
          69.0      43.4
          70.0      14.7
          71.0      36.9
          72.0       2.2
          75.0       1.5
          76.0       1.0
          77.0       2.1
          78.0       7.4
          79.0      56.6
          80.0       6.5
          81.0       1.8
          82.0       3.1
          83.0      20.6
          84.0       9.0
          85.0      17.5
          86.0       1.2
          91.0      83.9
          92.0       4.2
          93.0      27.5
          94.0       2.0
          95.0       1.0
          96.0       1.2
          97.0      11.9
          98.0       4.4
          99.0       1.5
         104.0       2.0
         105.0      22.2
         106.0       3.1
         107.0       7.7
         111.0       4.2
         112.0       1.9
         119.0       5.0
         121.0       1.5
         133.0       1.8
         147.0       1.0
         248.0       7.8
         249.0       2.5
         274.0       2.7
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C17 H30 Cl N 0.033 g : 0.5 ml CDCl3
    1-dodecylpyridinium chloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.543 B 8.544 C 8.208 D 4.979 E 2.040 F 1.33 G 1.22 J 0.871

         Hz     ppm     Int.
    

       3816.68   9.551    198
       3811.04   9.536    200
       3426.97   8.575     57
       3419.04   8.556    121
       3411.25   8.536     72
       3287.20   8.226    132
       3280.64   8.209    175
       3279.88   8.207    170
       3273.01   8.190    122
       1997.68   4.999    123
       1990.36   4.981    211
       1982.88   4.962    132
        822.91   2.060     68
        815.58   2.041    102
        808.26   2.023     80
        800.63   2.004     33
        530.40   1.328    157
        507.66   1.271    170
        501.86   1.256    262
        489.35   1.225   1000
        355.22   0.889    225
        348.36   0.872    622
        341.34   0.855    268
    

in CDCl3



CCl4 solution



KBr disc



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