-
MassMS-NW-9414 9,10-bis(chloromethyl)anthracene C16H12Cl2 (Mass of molecular ion: 274)
Source Temperature: 220 °C Sample Temperature: 150 °C Direct, 75 eV
17.0 1.2 18.0 6.4 36.0 6.7 38.0 2.2 39.0 1.3 50.0 1.2 51.0 1.9 62.0 1.1 63.0 3.0 74.0 1.8 75.0 4.4 76.0 6.6 77.0 1.0 87.0 3.2 87.5 1.0 88.0 12.3 88.5 1.9 89.0 8.5 89.5 1.2 91.0 2.3 92.0 1.6 94.5 1.8 99.0 1.3 100.0 8.6 100.5 4.0 101.0 28.3 101.5 7.2 102.0 7.8 102.5 1.2 119.0 2.5 119.5 1.1 126.0 1.0 150.0 2.6 151.0 2.4 152.0 2.3 163.0 1.6 165.0 1.2 174.0 1.5 175.0 1.7 176.0 4.8 177.0 1.7 178.0 2.5 187.0 1.3 188.0 1.0 189.0 4.3 191.0 1.1 199.0 1.3 200.0 9.9 201.0 10.3 202.0 50.7 203.0 49.4 204.0 100.0 205.0 17.1 206.0 1.7 238.0 3.2 239.0 58.3 240.0 11.2 241.0 19.7 242.0 3.3 274.0 18.1 275.0 3.2 276.0 11.9 277.0 2.1 278.0 2.0
400 MHz in DMSO-d6
-
1H NMR 399.65 MHz C16 H12 Cl2 saturated in DMSO-d6 9,10-bis(chloromethyl)anthracene 
Assign. Shift(ppm)
A 8.522 B 7.726 C 5.880
Hz ppm Int.3415.28 8.546 41 3414.06 8.543 51 3411.38 8.536 373 3408.20 8.528 288 3404.54 8.519 287 3401.25 8.511 419 3398.56 8.504 66 3397.46 8.502 51 3096.68 7.749 46 3095.58 7.746 60 3092.90 7.740 428 3089.60 7.731 326 3085.94 7.722 326 3082.76 7.714 428 3080.08 7.707 62 3078.98 7.705 44 2350.22 5.881 1000
in DMSO-d6
KBr disc
nujol mull
更多供应商
