1,2-环氧基-5-己烯

Mass

MS-IW-1524          
5,6-epoxy-1-hexene
C6H10O              (Mass of molecular ion:     98)

   Source Temperature: 250 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       4.8
      26.0       4.1
      27.0      43.8
      28.0       9.0
      29.0      52.7
      30.0       1.3
      31.0      63.7
      37.0       2.2
      38.0       6.0
      39.0      72.0
      40.0      22.7
      41.0      87.1
      42.0      38.2
      43.0      18.0
      44.0      12.1
      45.0       2.0
      50.0       3.6
      51.0       5.1
      52.0       3.2
      53.0      38.8
      54.0      91.0
      55.0      68.8
      56.0      13.8
      57.0      42.1
      58.0       3.1
      62.0       1.0
      63.0       1.6
      65.0      11.0
      66.0       5.6
      67.0     100.0
      68.0      49.8
      69.0      26.7
      70.0      11.4
      71.0       4.4
      77.0       1.8
      79.0      12.7
      80.0       7.8
      81.0       2.4
      83.0      15.9
      97.0       6.9
     147.0       1.7

Assign. Shift(ppm) A 5.841 B 5.062 C 4.990 D 2.927 E 2.741 F 2.474 G 2.220 J 1.631 J(A,B)=17.0HZ J(A,C)=10.1HZ J(A,G)=6.7HZ J(D,E)=3.6HZ J(D,F)=2.8HZ J(E,F)=-5.2HZ

     Hz     ppm     Int.

   2355.22   5.894    198
   2348.51   5.877    386
   2345.09   5.868    221
   2342.04   5.861    218
   2338.26   5.851    560
   2331.54   5.834    579
   2327.88   5.825    238
   2324.83   5.818    233
   2321.29   5.809    441
   2314.70   5.792    231
   2033.57   5.089    352
   2031.98   5.085    717
   2030.03   5.080    793
   2028.44   5.076    364
   2016.48   5.046    324
   2014.89   5.042    650
   2012.94   5.037    745
   2011.35   5.033    342
   2001.34   5.008    364
   2000.12   5.005    681
   1999.51   5.004    551
   1998.90   5.002    532
   1998.17   5.000    639
   1996.95   4.997    335
   1991.21   4.983    333
   1989.99   4.980    617
   1989.38   4.978    521
   1988.77   4.977    495
   1988.04   4.975    625
   1986.82   4.972    320
   1178.71   2.950    224
   1176.03   2.943    256
   1174.80   2.940    297
   1173.58   2.937    294
   1172.24   2.934    407
   1170.78   2.930    317
   1169.68   2.927    470
   1168.95   2.925    361
   1166.87   2.920    393
   1166.26   2.919    334
   1164.79   2.915    282
   1163.45   2.912    282
   1160.77   2.905    251
   1099.73   2.752    861
   1095.83   2.742    862
   1094.73   2.740   1000
   1090.70   2.730    810
    992.68   2.484    910
    989.87   2.477    860
    987.55   2.472    806
    984.86   2.465    774
    915.77   2.292     42
    914.31   2.288     34
    910.16   2.278     52
    908.94   2.275     89
    907.71   2.272     77
    905.15   2.265     42
    902.47   2.259    182
    901.12   2.255    254
    899.78   2.252    177
    896.97   2.245    186
    895.75   2.242    398
    894.41   2.238    543
    893.19   2.235    433
    891.72   2.232    229
    888.67   2.224    561
    887.45   2.221    654
    886.23   2.218    543
    883.06   2.210    212
    881.84   2.207    442
    880.49   2.204    563
    879.27   2.201    440
    875.12   2.190    177
    873.78   2.187    262
    872.44   2.184    185
    868.41   2.173     48
    867.19   2.170     77
    865.97   2.167     95
    864.75   2.164     62
    860.47   2.154     37
    859.13   2.150     49
    857.79   2.147     36
    678.10   1.697     72
    672.97   1.684     89
    671.02   1.680     90
    669.80   1.676     69
    665.89   1.667    131
    664.18   1.662    425
    659.18   1.650    597
    656.25   1.643    507
    652.95   1.634    581
    651.73   1.631    707
    648.93   1.624    414
    646.00   1.617    501
    643.92   1.612    514
    638.43   1.598    337
    632.81   1.584     66
    631.35   1.580     98
    624.51   1.563     56