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MS-NW-3756 2-pyridineethanol C7H9NO (Mass of molecular ion: 123)
Source Temperature: 200 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 1.0 18.0 2.4 26.0 2.8 27.0 5.5 28.0 4.0 29.0 2.4 31.0 9.2 37.0 1.8 38.0 3.5 39.0 17.1 40.0 4.1 41.0 3.2 42.0 1.5 50.0 5.6 51.0 12.0 52.0 14.1 53.0 5.0 54.0 1.6 62.0 1.2 63.0 3.6 64.0 2.7 65.0 18.9 66.0 18.9 67.0 5.2 77.0 2.1 78.0 11.7 79.0 43.1 80.0 9.5 92.0 14.1 93.0 100.0 94.0 13.0 104.0 7.1 105.0 19.0 106.0 89.8 107.0 7.2 108.0 1.1 122.0 25.0 123.0 14.1 124.0 1.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H9 N O 0.04 ml : 0.5 ml CDCl3 2-pyridineethanol Assign. Shift(ppm)
A 8.449 B 7.589 C 7.16 D 7.14 E 4.59 F 3.994 G 3.010
Hz ppm Int.
760.75 8.495 130 759.63 8.482 164 758.94 8.475 178 758.00 8.464 158 756.00 8.442 142 754.88 8.429 167 753.94 8.419 178 753.06 8.409 169 689.63 7.701 122 687.75 7.680 123 682.38 7.620 168 681.56 7.611 193 680.31 7.597 215 679.88 7.592 217 674.38 7.530 258 672.50 7.509 247 647.19 7.227 92 645.88 7.212 355 645.38 7.207 265 644.69 7.199 316 644.06 7.192 321 642.75 7.177 108 639.31 7.139 278 637.88 7.123 313 637.38 7.117 272 636.88 7.112 288 635.56 7.097 122 631.94 7.057 130 631.50 7.052 92 631.06 7.047 84 630.69 7.043 111 411.00 4.590 354 364.13 4.066 444 358.19 4.000 1000 353.50 3.948 66 352.25 3.934 620 275.13 3.073 392 269.19 3.006 615 263.38 2.941 299
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