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MS-NW-1310 N-methylbenzylamine C8H11N (Mass of molecular ion: 121)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 3.7 18.0 2.2 27.0 2.8 28.0 14.4 29.0 1.0 30.0 28.2 38.0 2.0 39.0 11.6 40.0 1.1 41.0 3.5 42.0 45.4 43.0 12.6 44.0 100.0 45.0 2.7 50.0 5.3 51.0 11.4 52.0 3.5 53.0 1.2 58.0 9.2 58.5 2.2 59.5 1.5 60.5 1.8 62.0 2.1 63.0 6.3 64.0 1.9 65.0 16.4 66.0 1.2 74.0 1.2 75.0 1.1 76.0 1.4 77.0 11.0 78.0 7.6 79.0 6.0 89.0 5.1 90.0 2.2 91.0 63.3 92.0 13.5 93.0 1.1 104.0 3.9 105.0 1.1 106.0 6.0 107.0 3.6 108.0 1.9 117.0 1.0 118.0 5.6 119.0 2.2 120.0 98.6 121.0 61.7 122.0 5.3 134.0 2.6 135.0 4.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H11 N 0.04 ml : 0.5 ml CDCl3 N-methylbenzylamine Assign. Shift(ppm)
A 7.50 to 7.10 B 3.741 C 2.434 D 2.20
Hz ppm Int.
660.44 7.375 32 659.25 7.361 39 658.69 7.355 37 656.69 7.333 110 655.94 7.325 146 653.88 7.302 891 651.94 7.280 161 651.31 7.273 188 649.06 7.248 91 335.00 3.741 449 218.00 2.435 1000 197.00 2.200 232
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