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MS-NW-1642 4,4'-dithiodimorpholine C8H16N2O2S2 (Mass of molecular ion: 236)
Source Temperature: 180 °C Sample Temperature: 120 °C Direct, 75 eV
15.0 7.7 18.0 2.0 26.0 3.3 27.0 13.6 28.0 41.7 29.0 21.8 30.0 15.6 31.0 4.8 32.0 1.7 40.0 1.1 41.0 4.8 42.0 17.0 43.0 2.9 44.0 6.2 45.0 1.9 46.0 2.2 47.0 2.1 54.0 7.8 55.0 30.1 56.0 87.0 57.0 20.8 58.0 2.6 59.0 4.5 60.0 27.9 61.0 6.2 62.0 2.4 64.0 12.8 66.0 1.3 72.0 1.8 74.0 3.5 84.0 14.2 85.0 18.6 86.0 100.0 87.0 21.3 88.0 9.6 89.0 1.8 90.0 2.9 116.0 45.3 117.0 3.3 118.0 55.6 119.0 3.5 120.0 2.7 149.0 42.5 150.0 54.8 151.0 15.6 152.0 5.6 153.0 1.2 236.0 26.5 237.0 3.0 238.0 2.6
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H16 N2 O2 S2 0.044 g : 0.5 ml CDCl3 4,4'-dithiodimorpholine Assign. Shift(ppm)
A 3.735 B 2.830
Hz ppm Int.
339.50 3.791 806 336.31 3.756 493 334.94 3.740 864 332.81 3.717 528 330.06 3.686 1000 326.00 3.641 44 325.31 3.633 40 260.56 2.910 36 257.81 2.879 801 255.00 2.848 403 252.94 2.825 717 251.63 2.810 413 250.00 2.792 135 248.38 2.774 649
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