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MS-NW-6830 ethyl p-(dimethylamino)benzoate C11H15NO2 (Mass of molecular ion: 193)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 1.7 18.0 1.6 26.0 1.0 27.0 3.5 28.0 1.7 29.0 2.7 39.0 2.3 42.0 9.9 43.0 1.3 44.0 2.3 50.0 3.6 51.0 3.8 52.0 1.5 58.5 1.6 59.5 2.4 63.0 3.0 64.0 1.2 65.0 3.1 66.0 1.0 73.5 10.4 74.0 5.1 75.0 1.6 76.0 3.1 77.0 10.9 78.0 4.9 79.0 5.0 90.0 2.2 91.0 4.2 92.0 2.4 93.0 1.5 103.0 1.6 104.0 6.6 105.0 8.0 106.0 1.1 118.0 4.1 119.0 4.3 120.0 8.2 121.0 6.3 132.0 3.5 148.0 100.0 149.0 13.8 150.0 2.1 164.0 41.6 165.0 24.4 166.0 2.6 178.0 1.3 192.0 12.7 193.0 92.6 194.0 11.9 195.0 1.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C11 H15 N O2 0.040 g : 0.5 ml CDCl3 ethyl p-(dimethylamino)benzoate Assign. Shift(ppm)
A 7.911 B 6.630 C 4.315 D 3.015 E 1.360
Hz ppm Int.
3169.07 7.930 22 3166.26 7.923 175 3164.18 7.918 55 3159.30 7.906 58 3157.10 7.900 179 3154.30 7.893 22 2657.35 6.650 21 2654.42 6.642 155 2652.34 6.637 49 2647.46 6.625 50 2645.39 6.620 149 1735.47 4.343 63 1728.27 4.325 187 1721.19 4.307 191 1714.11 4.290 65 1204.96 3.016 1000 550.66 1.378 197 543.46 1.360 371 536.38 1.343 193
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