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2′-CHLORO-5′-METHYLBENZANILIDE

产品名称 2′-CHLORO-5′-METHYLBENZANILIDE

CAS号10286-87-0

分子式C14H12ClNO

分子量245.7


  • Mass

    MS-IW-0003          
    2'-chloro-5'-methylbenzanilide
    C14H12ClNO          (Mass of molecular ion:    245)
    

       Source Temperature: 140 °C
       Sample Temperature: 100 °C
       Direct, 75 eV
    

          50.0       1.7
          51.0       8.6
          52.0       1.0
          76.0       1.8
          77.0      46.5
          78.0       3.9
         104.0       1.0
         105.0     100.0
         106.0       8.1
         210.0      63.2
         211.0      10.1
         245.0      14.5
         246.0       2.4
         247.0       4.9
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C14 H12 Cl N O 0.036 g : 0.5 ml CDCl3
    2'-chloro-5'-methylbenzanilide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.400 B 7.910 C 7.564 D 7.507 E 7.266 F 6.883 G 2.365

         Hz     ppm     Int.
    

       3357.06   8.401    238
       3355.47   8.397    224
       3165.89   7.922    250
       3164.31   7.918    141
       3160.89   7.910     96
       3158.81   7.904    301
       3157.35   7.901    219
       3032.71   7.589     46
       3031.49   7.586     32
       3028.08   7.577     40
       3025.39   7.571    155
       3023.07   7.565     55
       3019.41   7.556     92
       3018.19   7.553    141
       3016.85   7.549     80
       3007.20   7.525    226
       3005.86   7.522    115
       3001.10   7.510    172
       2999.51   7.506    289
       2994.14   7.492     60
       2992.55   7.488    115
       2991.21   7.485     73
       2908.20   7.277    219
       2900.02   7.257    253
       2755.49   6.895    106
       2753.91   6.891    105
       2747.31   6.875     97
       2745.73   6.871     94
        945.43   2.366   1000
    

in CDCl3



KBr disc



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