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网站主页CAS数据库列表 10229-11-5更多图谱4-苯基-3-丁炔-1-醇(10229-11-5)核磁图(13CNMR)

4-苯基-3-丁炔-1-醇

产品名称 4-苯基-3-丁炔-1-醇

CAS号10229-11-5

分子式C10H10O

分子量146.19

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  • Mass

    MS-IW-4781          
    4-phenyl-3-butyn-1-ol
    C10H10O             (Mass of molecular ion:    146)
    

       Source Temperature: 210 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          18.0       1.1
          28.0       1.1
          31.0       3.1
          39.0       3.8
          50.0       2.4
          51.0       4.4
          62.0       2.6
          63.0       7.7
          64.0       1.6
          65.0       4.8
          74.0       2.2
          75.0       2.7
          76.0       1.8
          77.0       3.6
          78.0       1.4
          86.0       1.1
          87.0       1.7
          88.0       1.8
          89.0       9.1
          90.0       1.0
          91.0       1.8
         102.0       4.9
         103.0       1.3
         105.0       3.0
         113.0       2.1
         114.0       3.0
         115.0     100.0
         116.0      46.4
         117.0       7.4
         118.0       1.8
         126.0       1.3
         127.0       4.8
         128.0      17.6
         129.0       2.8
         131.0       1.7
         145.0       4.6
         146.0      45.4
         147.0       5.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10 H10 O 0.05 ml : 0.5 ml CDCl3
    4-phenyl-3-butyn-1-ol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.407 B 7.26 C 3.775 D 3.37 E 2.644

         Hz     ppm     Int.
    

       2969.36   7.430     42
       2965.33   7.420    288
       2963.75   7.416    209
       2962.16   7.412    292
       2961.30   7.410    292
       2959.96   7.407    296
       2958.50   7.403    325
       2957.28   7.400    254
       2955.69   7.396    364
       2951.66   7.386     70
       2909.91   7.282     41
       2907.10   7.275    119
       2906.49   7.273    124
       2905.27   7.270    257
       2904.79   7.269    255
       2903.44   7.265    727
       2901.98   7.262    397
       2901.25   7.260    443
       2900.15   7.257    718
       2899.05   7.254    426
       2896.97   7.249    685
       2895.63   7.246    205
       2892.94   7.239     88
       2892.58   7.238     87
       1515.14   3.792    491
       1508.67   3.775   1000
       1502.20   3.759    487
       1346.68   3.370     61
       1062.99   2.660    429
       1056.52   2.644    818
       1050.05   2.628    394
    

in CDCl3



liquid film