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MS-NW-1819 2,2'-(butylimino)diethanol C8H19NO2 (Mass of molecular ion: 161)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 10.0 17.0 2.1 18.0 10.0 19.0 5.1 26.0 1.8 27.0 20.8 28.0 15.5 29.0 41.1 30.0 36.1 31.0 7.2 39.0 7.0 40.0 1.2 41.0 33.5 42.0 41.2 43.0 11.4 44.0 27.9 45.0 29.7 53.0 1.4 54.0 2.6 55.0 6.3 56.0 64.1 57.0 21.4 58.0 6.3 60.0 1.9 68.0 1.1 70.0 5.2 72.0 3.3 73.0 1.5 74.0 58.9 75.0 2.5 84.0 3.2 86.0 10.8 87.0 1.0 88.0 100.0 89.0 4.9 98.0 4.4 100.0 4.0 104.0 1.2 114.0 1.4 116.0 6.0 118.0 27.8 119.0 1.8 128.0 2.2 130.0 97.8 131.0 8.5 160.0 1.0 161.0 1.4 174.0 1.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H19 N O2 0.05 ml : 0.5 ml CDCl3 2,2'-(butylimino)diethanol Assign. Shift(ppm)
A 3.96 B 3.599 C 2.636 D 2.521 E 1.444 F 1.306 G 0.917
Hz ppm Int.
1583.74 3.963 176 1443.60 3.613 597 1438.35 3.600 855 1432.74 3.585 586 1427.49 3.572 33 1058.84 2.650 605 1053.34 2.636 805 1047.85 2.622 536 1015.14 2.541 299 1007.57 2.522 285 1005.98 2.518 164 999.88 2.502 302 593.99 1.487 56 586.91 1.469 132 584.11 1.462 110 581.05 1.454 112 578.61 1.448 204 575.56 1.441 102 573.49 1.435 108 571.17 1.430 157 568.97 1.424 118 563.72 1.411 88 539.67 1.351 57 532.59 1.333 160 525.27 1.315 218 517.21 1.295 199 510.01 1.277 124 502.81 1.259 41 373.66 0.935 555 366.46 0.917 1000 359.13 0.899 453 355.35 0.890 30
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