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MS-NW-0800 triallylamine C9H15N (Mass of molecular ion: 137)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.0 26.0 1.1 27.0 7.4 28.0 4.5 29.0 6.9 30.0 2.4 38.0 2.1 39.0 28.0 40.0 4.3 41.0 90.9 42.0 30.9 43.0 23.7 44.0 1.4 45.0 13.5 51.0 1.4 52.0 1.3 53.0 3.3 54.0 7.9 55.0 11.3 56.0 25.4 57.0 15.9 58.0 1.0 65.0 1.1 67.0 6.8 68.0 14.7 69.0 5.9 70.0 7.0 71.0 7.5 77.0 1.3 78.0 3.6 79.0 4.8 80.0 3.3 81.0 11.8 82.0 4.5 83.0 2.8 84.0 2.6 85.0 1.7 86.0 2.1 91.0 1.8 92.0 1.0 93.0 1.0 94.0 8.4 95.0 3.8 96.0 13.9 97.0 1.3 105.0 1.0 108.0 11.4 109.0 2.3 110.0 100.0 111.0 8.9 120.0 1.2 122.0 7.8 136.0 9.3 137.0 23.8 138.0 2.7
parameter in CDCl3
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1H NMR 300 MHz C9 H15 N 10.5 mol% in CDCl3 triallylamine Parameter ppm Hz
D(A) 5.236 D(B) 4.627 D(C) 4.595 D(D) 2.760 J(A,B) 17.20 J(A,C) 10.21 J(A,D) 6.50 J(B,C) 2.02 J(B,D) -1.38 J(C,D) -1.23
Hz ppm Int.
1591.53 5.305 102 1585.05 5.283 205 1581.35 5.271 116 1578.57 5.262 110 1574.85 5.249 266 1567.89 5.226 281 1564.19 5.214 141 1561.39 5.205 131 1557.69 5.192 273 1551.23 5.171 141 1398.79 4.663 133 1397.42 4.658 273 1396.76 4.656 255 1395.41 4.651 364 1394.03 4.647 187 1385.60 4.619 188 1384.36 4.615 354 1383.20 4.611 276 1382.33 4.608 287 1381.59 4.605 203 1381.17 4.604 205 1380.23 4.601 243 1379.56 4.599 230 1378.20 4.594 326 1376.85 4.589 186 1375.42 4.585 191 1374.19 4.581 334 1373.03 4.577 247 1372.18 4.574 222 1370.97 4.570 113 832.49 2.775 570 831.24 2.771 1000 829.96 2.767 569 826.04 2.753 564 824.76 2.749 982 823.48 2.745 553
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