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MassMS2014-05015CW p-(p-nitrophenylthio)aniline C12H10N2O2S (Mass of molecular ion: 246)
Source Temperature: 250 °C Sample Temperature: 25 °C Direct, 70 eV
39.0 1.2 53.0 1.0 63.0 1.6 65.0 2.4 69.0 1.0 80.0 7.2 97.0 1.5 99.5 4.1 100.0 1.1 123.0 2.0 124.0 23.7 125.0 2.3 126.0 1.3 139.0 3.3 140.0 1.0 154.0 1.1 156.0 1.2 166.0 1.2 167.0 10.1 168.0 1.8 171.0 3.5 172.0 1.6 183.0 6.0 184.0 6.4 185.0 1.2 188.0 2.1 198.0 1.9 199.0 18.2 200.0 24.2 201.0 4.3 202.0 1.3 214.0 1.4 216.0 5.8 230.0 1.0 245.0 3.2 246.0 100.0 247.0 14.4 248.0 5.9
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C12 H10 N2 O2 S 0.033 g : 0.5 ml DMSO-d6 p-(p-nitrophenylthio)aniline 
Assign. Shift(ppm)
A 8.096 B 7.240 C 7.149 D 6.709 E 5.75
Hz ppm Int.3242.92 8.115 130 3240.23 8.108 966 3238.16 8.103 311 3233.15 8.090 329 3231.20 8.086 1000 3228.52 8.079 136 2901.00 7.259 111 2898.19 7.252 842 2896.24 7.247 284 2891.60 7.236 310 2889.65 7.231 917 2886.84 7.224 129 2864.50 7.168 143 2861.69 7.161 997 2859.62 7.156 317 2857.18 7.150 70 2854.74 7.144 328 2852.66 7.138 955 2849.98 7.132 131 2688.35 6.727 125 2685.67 6.721 953 2683.59 6.715 303 2678.96 6.704 308 2677.00 6.699 882 2674.19 6.692 119 2296.26 5.746 795
in DMSO-d6
KBr disk
Nujol
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