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MS-NW-1460 2,4,6-tris(allyloxy)-1,3,5-triazine C12H15N3O3 (Mass of molecular ion: 249)
Source Temperature: 250 °C Sample Temperature: 170 °C Reservoir, 75 eV
15.0 1.6 18.0 1.0 27.0 3.0 28.0 3.9 29.0 1.3 38.0 1.1 39.0 24.6 40.0 3.4 41.0 100.0 42.0 4.9 43.0 1.1 44.0 1.1 54.0 5.4 55.0 5.0 56.0 6.8 57.0 4.5 67.0 3.3 68.0 1.8 69.0 6.3 70.0 13.7 79.0 4.3 80.0 9.3 81.0 4.9 82.0 34.9 83.0 20.9 84.0 8.2 87.0 1.7 94.0 1.3 95.0 1.2 96.0 1.9 97.0 1.2 99.0 1.3 109.0 3.4 110.0 1.4 111.0 2.2 112.0 2.4 113.0 1.0 123.0 1.1 124.0 1.8 125.0 10.8 126.0 1.6 127.0 2.2 137.0 1.1 138.0 1.1 139.0 1.2 151.0 1.6 152.0 1.4 153.0 1.0 165.0 1.2 166.0 1.1 167.0 1.3 170.0 1.1 192.0 1.5 193.0 3.1 195.0 1.7 207.0 1.0 208.0 6.9 209.0 1.2 234.0 1.0 249.0 1.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C12 H15 N3 O3 0.04 ml : 0.5 ml CDCl3 2,4,6-tris(allyloxy)-1,3,5-triazine Assign. Shift(ppm)
A 6.04 B 5.40 C 5.30 D 4.913
Hz ppm Int.
562.81 6.285 98 557.06 6.220 193 552.63 6.171 131 551.50 6.158 122 546.94 6.107 223 545.63 6.093 173 541.50 6.047 153 539.81 6.028 300 535.50 5.980 214 534.38 5.967 217 530.06 5.919 261 529.69 5.915 362 524.38 5.856 265 494.69 5.524 182 493.25 5.508 484 491.56 5.489 641 490.19 5.474 271 480.56 5.366 230 479.38 5.353 537 478.75 5.346 253 478.19 5.340 334 477.69 5.334 469 476.56 5.322 246 476.00 5.315 341 474.56 5.299 309 473.00 5.282 163 470.50 5.254 142 469.25 5.240 352 468.75 5.234 188 468.00 5.226 253 467.56 5.221 336 466.44 5.209 188 443.94 4.957 690 442.75 4.944 1000 441.44 4.929 633 438.50 4.897 492 437.06 4.881 973 435.75 4.866 625
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