4,4'-二(苯基异丙基)二苯胺

Mass

MS-KW-0228          
4,4'-bis(alpha,alpha-dimethylbenzyl)diphenylamine
C30H31N             (Mass of molecular ion:    405)

   Source Temperature: 190 °C
   Sample Temperature: 170 °C
   Direct, 75 eV

      18.0       2.3
      27.0       1.6
      28.0       1.2
      39.0       6.6
      41.0       4.4
      50.0       3.6
      51.0      11.3
      52.0       2.6
      57.0       1.3
      57.5       3.2
      58.0       5.2
      62.0       1.2
      63.0       4.1
      64.0       1.2
      65.0       6.9
      66.0       2.9
      71.5       1.0
      74.0       1.5
      75.0       1.7
      76.0       2.3
      77.0      21.4
      78.0      18.6
      79.0       3.2
      83.5       4.8
      84.0       1.2
      84.5       1.2
      89.0       3.5
      90.0       1.9
      91.0      20.5
      92.0       7.9
      93.0       1.4
     101.0       1.0
     102.0       4.5
     103.0      48.8
     103.5       2.7
     104.0       5.8
     105.0       1.4
     108.5       1.2
     109.5       7.7
     110.0       1.6
     115.0      15.2
     116.0       5.3
     117.0      42.4
     118.0      53.8
     119.0      20.1
     120.0       2.1
     127.0       2.3
     127.5       2.7
     128.0       2.9
     128.5       3.6
     129.0       1.8
     130.0       1.4
     132.0       1.0
     134.5       1.3
     135.0       1.0
     135.5       1.6
     136.0      11.5
     136.5       1.9
     139.0       1.8
     140.0       1.6
     140.5       1.0
     141.0       3.8
     142.0       1.3
     143.0       1.4
     143.5       2.0
     147.0       1.2
     148.0       4.5
     148.5       9.3
     149.0       3.3
     152.0       3.2
     153.0       2.0
     154.0       1.3
     156.0       1.0
     156.5       1.0
     165.0       9.5
     166.0       4.3
     167.0      13.7
     168.0      17.2
     169.0      28.6
     170.0       5.8
     177.0       1.4
     178.0       6.6
     179.0       7.7
     180.0      12.9
     181.0       2.5
     182.0       1.1
     187.0      23.8
     187.5      12.5
     191.0       1.2
     192.0       1.4
     193.0       2.7
     194.0       7.3
     195.0       5.9
     202.0       1.4
     209.0       1.3
     210.0       8.7
     211.0       1.5
     254.0       1.5
     256.0       2.2
     257.0       1.0
     270.0       1.7
     271.0       4.8
     272.0     100.0
     273.0      22.5
     274.0       2.5
     286.0       1.0
     287.0      48.0
     288.0      11.7
     289.0       1.3
     296.0       1.0
     298.0       2.6
     312.0       2.5
     313.0       1.0
     328.0       6.1
     329.0       1.6
     374.0       8.2
     375.0       5.1
     376.0       1.6
     390.0      65.8
     391.0      21.5
     392.0       3.5
     405.0      43.7
     406.0      14.3
     407.0       2.4

Assign. Shift(ppm) A 7.25 B 7.15 C 7.087 D 6.932 E 5.53 F 1.651

     Hz     ppm     Int.

   2908.70   7.276     20
   2908.21   7.275     19
   2907.48   7.273     19
   2905.89   7.269     19
   2902.47   7.261     38
   2899.66   7.254    276
   2898.69   7.251    294
   2895.02   7.242    686
   2891.36   7.233     24
   2889.90   7.229     35
   2870.37   7.180     37
   2865.73   7.169     48
   2862.43   7.160     44
   2861.82   7.159     46
   2861.09   7.157     45
   2860.48   7.156     40
   2857.18   7.147     59
   2855.96   7.144     34
   2854.50   7.141     28
   2853.15   7.137     25
   2852.06   7.135     47
   2848.64   7.126     23
   2841.07   7.107     24
   2838.26   7.100    172
   2836.06   7.095     60
   2831.67   7.084     69
   2829.47   7.078    221
   2826.67   7.071     28
   2777.71   6.949     33
   2775.03   6.942    222
   2772.83   6.936     65
   2768.32   6.925     60
   2766.24   6.920    167
   2763.31   6.913     19
   2211.80   5.533     45
    660.04   1.651   1000